Chromatography analysis and thermal stability of hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole

Ke Jian Cui; Zi Hui Meng; Zhi Bin Xu; Min Xue; Bo Zhou Wang; Zhong Xue Ge; Guang Ming Qin; Zhi Hui Lin

Chromatography analysis and thermal stability of hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole

Ke Jian Cui, Zi Hui Meng^*, Zhi Bin Xu, Min Xue, Bo Zhou Wang, Zhong Xue Ge, Guang Ming Qin, Zhi Hui Lin

^*Corresponding author for this work

School of Chemistry and Chemical Engineering

Research output: Contribution to journal › Article › peer-review

2 Citations (Scopus)

Abstract

A high performance liquid chromatography (HPLC) method was developed for the analysis of hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole (HDNAT) and the anions and cations in crude HDNAT were determined by ion chromatography (IC). The thermal stability of HDNAT was investigated by TG-DTA and DSC. The result shows that there are CH₃COO^-, Na⁺, NH₄⁺, K⁺, Mg²⁺ and Ca²⁺ in the HDNAT sample. Its initial decomposition temperature is 183°C, and decomposition heat is 589.14 J/g.

Original language	English
Pages (from-to)	35-38
Number of pages	4
Journal	Huozhayao Xuebao/Chinese Journal of Explosives and Propellants
Volume	36
Issue number	3
Publication status	Published - Jun 2013

Keywords

Analytical chemistry
HDNAT
HPLC
High performance liquid chromatography
Hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole
Ion chromatography
Thermal stability

Cite this

@article{6b061d9d8cd0451db09f9620d3f3012e,

title = "Chromatography analysis and thermal stability of hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole",

abstract = "A high performance liquid chromatography (HPLC) method was developed for the analysis of hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole (HDNAT) and the anions and cations in crude HDNAT were determined by ion chromatography (IC). The thermal stability of HDNAT was investigated by TG-DTA and DSC. The result shows that there are CH3COO-, Na+, NH4+, K+, Mg2+ and Ca2+ in the HDNAT sample. Its initial decomposition temperature is 183°C, and decomposition heat is 589.14 J/g.",

keywords = "Analytical chemistry, HDNAT, HPLC, High performance liquid chromatography, Hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole, Ion chromatography, Thermal stability",

author = "Cui, {Ke Jian} and Meng, {Zi Hui} and Xu, {Zhi Bin} and Min Xue and Wang, {Bo Zhou} and Ge, {Zhong Xue} and Qin, {Guang Ming} and Lin, {Zhi Hui}",

year = "2013",

month = jun,

language = "English",

volume = "36",

pages = "35--38",

journal = "Huozhayao Xuebao/Chinese Journal of Explosives and Propellants",

issn = "1007-7812",

publisher = "China Ordnance Industry Corporation",

number = "3",

}

TY - JOUR

T1 - Chromatography analysis and thermal stability of hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole

AU - Cui, Ke Jian

AU - Meng, Zi Hui

AU - Xu, Zhi Bin

AU - Xue, Min

AU - Wang, Bo Zhou

AU - Ge, Zhong Xue

AU - Qin, Guang Ming

AU - Lin, Zhi Hui

PY - 2013/6

Y1 - 2013/6

N2 - A high performance liquid chromatography (HPLC) method was developed for the analysis of hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole (HDNAT) and the anions and cations in crude HDNAT were determined by ion chromatography (IC). The thermal stability of HDNAT was investigated by TG-DTA and DSC. The result shows that there are CH3COO-, Na+, NH4+, K+, Mg2+ and Ca2+ in the HDNAT sample. Its initial decomposition temperature is 183°C, and decomposition heat is 589.14 J/g.

AB - A high performance liquid chromatography (HPLC) method was developed for the analysis of hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole (HDNAT) and the anions and cations in crude HDNAT were determined by ion chromatography (IC). The thermal stability of HDNAT was investigated by TG-DTA and DSC. The result shows that there are CH3COO-, Na+, NH4+, K+, Mg2+ and Ca2+ in the HDNAT sample. Its initial decomposition temperature is 183°C, and decomposition heat is 589.14 J/g.

KW - Analytical chemistry

KW - HDNAT

KW - HPLC

KW - High performance liquid chromatography

KW - Hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole

KW - Ion chromatography

KW - Thermal stability

UR - http://www.scopus.com/inward/record.url?scp=84883417104&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:84883417104

SN - 1007-7812

VL - 36

SP - 35

EP - 38

JO - Huozhayao Xuebao/Chinese Journal of Explosives and Propellants

JF - Huozhayao Xuebao/Chinese Journal of Explosives and Propellants

IS - 3

ER -

Chromatography analysis and thermal stability of hydrazonium salt of 3, 5-dinitroamine-1, 2, 4-triazole

Abstract

Keywords

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