TY - JOUR
T1 - Synthesis of 1, 5, 6, 10 - Tetranitrodecahydro - [1, 4] Diazepino [2, 3-b] Diazepine and Its Thermal Property Research
AU - Li, Sainan
AU - Meng, Zihui
AU - Xu, Zhibin
N1 - Publisher Copyright:
© Published under licence by IOP Publishing Ltd.
PY - 2018/8/8
Y1 - 2018/8/8
N2 - 1, 5, 6, 10 - tetranitrodecahydro- [1, 4] diazepino [2, 3-b] diazepine (TNDP) was synthesized using tetranitroglycoluril as the starting material by hydrolysis reaction and condensation. The thermo stability of TNDP was studied by DSC and TG-DTA methods, and the thermodynamic parameters were calculated by Kissinger method and related formulas. The results showed that TNDP was thermal stable and the peak temperature of DSC was 311.76 °C. The apparent activation energy was 162.70 kJ/mol. In general, TNDP is a kind of good performance energetic materials.
AB - 1, 5, 6, 10 - tetranitrodecahydro- [1, 4] diazepino [2, 3-b] diazepine (TNDP) was synthesized using tetranitroglycoluril as the starting material by hydrolysis reaction and condensation. The thermo stability of TNDP was studied by DSC and TG-DTA methods, and the thermodynamic parameters were calculated by Kissinger method and related formulas. The results showed that TNDP was thermal stable and the peak temperature of DSC was 311.76 °C. The apparent activation energy was 162.70 kJ/mol. In general, TNDP is a kind of good performance energetic materials.
UR - http://www.scopus.com/inward/record.url?scp=85052364487&partnerID=8YFLogxK
U2 - 10.1088/1757-899X/394/2/022014
DO - 10.1088/1757-899X/394/2/022014
M3 - Conference article
AN - SCOPUS:85052364487
SN - 1757-8981
VL - 394
JO - IOP Conference Series: Materials Science and Engineering
JF - IOP Conference Series: Materials Science and Engineering
IS - 2
M1 - 022014
T2 - 2018 5th International Conference on Advanced Composite Materials and Manufacturing Engineering, ACMME 2018
Y2 - 16 June 2018 through 17 June 2018
ER -