Abstract
Ceramic powder Ba(Mg1/3Ta2/3)O3 (BMT) was synthesized by the solid-phase synthesis method with the raw materials powder of BaCO3, MgO, and Ta2O5. Then BMT/YSZ coatings were prepared by atmospheric plasma spraying (APS). The phase composition and microstructure of the BMT powder and coatings were analyzed by XRD, SEM and optical microscope. The thermal shock resistance was evaluated by water quenching. The results show that the BMT powder with perovskite structure can be synthesized at 1450 ℃ for 4 h. The BMT powder reveals desirable phase stability. The BMT/YSZ coatings have a compact microstructure and higher binding strength between each coating. Spallation is observed within the BMT coatings after 9 cycle thermal shock testing from 1150 ℃ to room temperature. Low fracture toughness of BMT and the precipitation of Ba3Ta5O15 phase are the main reasons for failure of BMT/YSZ coatings.
Translated title of the contribution | Preparation and Thermal Shock Resistance of Ba(Mg1/3Ta2/3)O3 Thermal Barrier Coatings |
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Original language | Chinese (Traditional) |
Pages (from-to) | 164-168 |
Number of pages | 5 |
Journal | Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering |
Volume | 47 |
Publication status | Published - 1 Jul 2018 |