Preparation and molecular structure of CHZNTO·H2O

Chang Gen Feng; Li Yang; Jian Guo Zhang; Tong Lai Zhang; Kai Bei Yu

Preparation and molecular structure of CHZNTO·H₂O

Chang Gen Feng^*, Li Yang, Jian Guo Zhang, Tong Lai Zhang, Kai Bei Yu

^*Corresponding author for this work

School of Mechatronical Engineering

Research output: Contribution to journal › Article › peer-review

13 Citations (Scopus)

Abstract

CHZNTO·H₂O was prepared by mixing carbohydrazide(CHZ) and 3-nitro-1, 2, 4-triazol-5-one (NTO). The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to triclinic, space group P1 with a = 6.639(1), b = 11.481(1), c = 13.692(2) Å, a = 70.56(1), β = 88.19(1), γ = 77.03 (1)°, V = 958(2)Å³, Z = 4, D_c = 1.651 g/cm³, μ(MoKα) = 0.150 mm ^-1. F(000) = 496, R = 0.0315 and wR = 0.0894. It is concluded that CHZNTO is an ionic compound composed of one CHZ cation and one NTO anion according to the crystal structure.

Original language	English
Pages (from-to)	309-312
Number of pages	4
Journal	Jiegou Huaxue
Volume	21
Issue number	3
Publication status	Published - 2002

Keywords

2,4-trinzol-5-one
3-nitro-1
Carbohydrazide
Crystal structure
Preparation

Cite this

@article{94cd3ecb1f4f48f3b7dc40f11862e200,

title = "Preparation and molecular structure of CHZNTO·H2O",

abstract = "CHZNTO·H2O was prepared by mixing carbohydrazide(CHZ) and 3-nitro-1, 2, 4-triazol-5-one (NTO). The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to triclinic, space group P1 with a = 6.639(1), b = 11.481(1), c = 13.692(2) {\AA}, a = 70.56(1), β = 88.19(1), γ = 77.03 (1)°, V = 958(2){\AA}3, Z = 4, Dc = 1.651 g/cm3, μ(MoKα) = 0.150 mm -1. F(000) = 496, R = 0.0315 and wR = 0.0894. It is concluded that CHZNTO is an ionic compound composed of one CHZ cation and one NTO anion according to the crystal structure.",

keywords = "2,4-trinzol-5-one, 3-nitro-1, Carbohydrazide, Crystal structure, Preparation",

author = "Feng, {Chang Gen} and Li Yang and Zhang, {Jian Guo} and Zhang, {Tong Lai} and Yu, {Kai Bei}",

year = "2002",

language = "English",

volume = "21",

pages = "309--312",

journal = "Jiegou Huaxue",

issn = "0254-5861",

publisher = "Fujian Institute of Research of the Structure of Matter",

number = "3",

}

TY - JOUR

T1 - Preparation and molecular structure of CHZNTO·H2O

AU - Feng, Chang Gen

AU - Yang, Li

AU - Zhang, Jian Guo

AU - Zhang, Tong Lai

AU - Yu, Kai Bei

PY - 2002

Y1 - 2002

N2 - CHZNTO·H2O was prepared by mixing carbohydrazide(CHZ) and 3-nitro-1, 2, 4-triazol-5-one (NTO). The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to triclinic, space group P1 with a = 6.639(1), b = 11.481(1), c = 13.692(2) Å, a = 70.56(1), β = 88.19(1), γ = 77.03 (1)°, V = 958(2)Å3, Z = 4, Dc = 1.651 g/cm3, μ(MoKα) = 0.150 mm -1. F(000) = 496, R = 0.0315 and wR = 0.0894. It is concluded that CHZNTO is an ionic compound composed of one CHZ cation and one NTO anion according to the crystal structure.

AB - CHZNTO·H2O was prepared by mixing carbohydrazide(CHZ) and 3-nitro-1, 2, 4-triazol-5-one (NTO). The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to triclinic, space group P1 with a = 6.639(1), b = 11.481(1), c = 13.692(2) Å, a = 70.56(1), β = 88.19(1), γ = 77.03 (1)°, V = 958(2)Å3, Z = 4, Dc = 1.651 g/cm3, μ(MoKα) = 0.150 mm -1. F(000) = 496, R = 0.0315 and wR = 0.0894. It is concluded that CHZNTO is an ionic compound composed of one CHZ cation and one NTO anion according to the crystal structure.

KW - 2,4-trinzol-5-one

KW - 3-nitro-1

KW - Carbohydrazide

KW - Crystal structure

KW - Preparation

UR - http://www.scopus.com/inward/record.url?scp=33845336550&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:33845336550

SN - 0254-5861

VL - 21

SP - 309

EP - 312

JO - Jiegou Huaxue

JF - Jiegou Huaxue

IS - 3

ER -

Preparation and molecular structure of CHZNTO·H₂O

Abstract

Keywords

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