Synthesis of [Pb(H2O)6][ATZ]·H2O and its impact on potassium nitrate decomposition temperature

Zhiyue Han; Li Gong; Zhiming Du; Wenchao Tong; Qi Jiang; Yu Wen

doi:10.1007/s10973-019-08864-8

Synthesis of [Pb(H₂O)₆][ATZ]·H₂O and its impact on potassium nitrate decomposition temperature

Zhiyue Han^*, Li Gong, Zhiming Du, Wenchao Tong, Qi Jiang, Yu Wen

^*此作品的通讯作者

机电学院

科研成果: 期刊稿件 › 文章 › 同行评审

2 引用（Scopus）

摘要

In this study, catalyst formation [Pb(H₂O)₆][ATZ]·H₂O (ATZ = azo tetrazolium anion) was successfully synthesized originally; meanwhile, the single-crystal structure of the compound was cultivated and analyzed by diffraction single-crystal method. The influence of the compound in which [Pb(H₂O)₆][ATZ]·H₂O was used as combustion catalyst on the decomposition temperature of potassium nitrate was studied by TG–DSC. The result proved that [Pb(H₂O)₆][ATZ]·H₂O can effectively reduce the decomposition temperature. In other words, [Pb(H₂O)₆][ATZ]·H₂O can reduce the decomposition temperature of potassium nitrate, so the addition of [Pb(H₂O)₆][ATZ]·H₂O can make potassium nitrate better to be used in the fields of initiating explosive device and fire engineering.

源语言	英语
页（从-至）	373-379
页数	7
期刊	Journal of Thermal Analysis and Calorimetry
卷	140
期	1
DOI	https://doi.org/10.1007/s10973-019-08864-8
出版状态	已出版 - 1 4月 2020

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@article{41054a70faae453a9c8daae88a899c46,

title = "Synthesis of [Pb(H2O)6][ATZ]·H2O and its impact on potassium nitrate decomposition temperature",

abstract = "In this study, catalyst formation [Pb(H2O)6][ATZ]·H2O (ATZ = azo tetrazolium anion) was successfully synthesized originally; meanwhile, the single-crystal structure of the compound was cultivated and analyzed by diffraction single-crystal method. The influence of the compound in which [Pb(H2O)6][ATZ]·H2O was used as combustion catalyst on the decomposition temperature of potassium nitrate was studied by TG–DSC. The result proved that [Pb(H2O)6][ATZ]·H2O can effectively reduce the decomposition temperature. In other words, [Pb(H2O)6][ATZ]·H2O can reduce the decomposition temperature of potassium nitrate, so the addition of [Pb(H2O)6][ATZ]·H2O can make potassium nitrate better to be used in the fields of initiating explosive device and fire engineering.",

keywords = "Decomposition temperature, Potassium nitrate, Single-crystal lattice, [Pb(HO)][ATZ]·HO",

author = "Zhiyue Han and Li Gong and Zhiming Du and Wenchao Tong and Qi Jiang and Yu Wen",

note = "Publisher Copyright: {\textcopyright} 2019, Akad{\'e}miai Kiad{\'o}, Budapest, Hungary.",

year = "2020",

month = apr,

day = "1",

doi = "10.1007/s10973-019-08864-8",

language = "English",

volume = "140",

pages = "373--379",

journal = "Journal of Thermal Analysis and Calorimetry",

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TY - JOUR

T1 - Synthesis of [Pb(H2O)6][ATZ]·H2O and its impact on potassium nitrate decomposition temperature

AU - Han, Zhiyue

AU - Gong, Li

AU - Du, Zhiming

AU - Tong, Wenchao

AU - Jiang, Qi

AU - Wen, Yu

PY - 2020/4/1

Y1 - 2020/4/1

N2 - In this study, catalyst formation [Pb(H2O)6][ATZ]·H2O (ATZ = azo tetrazolium anion) was successfully synthesized originally; meanwhile, the single-crystal structure of the compound was cultivated and analyzed by diffraction single-crystal method. The influence of the compound in which [Pb(H2O)6][ATZ]·H2O was used as combustion catalyst on the decomposition temperature of potassium nitrate was studied by TG–DSC. The result proved that [Pb(H2O)6][ATZ]·H2O can effectively reduce the decomposition temperature. In other words, [Pb(H2O)6][ATZ]·H2O can reduce the decomposition temperature of potassium nitrate, so the addition of [Pb(H2O)6][ATZ]·H2O can make potassium nitrate better to be used in the fields of initiating explosive device and fire engineering.

AB - In this study, catalyst formation [Pb(H2O)6][ATZ]·H2O (ATZ = azo tetrazolium anion) was successfully synthesized originally; meanwhile, the single-crystal structure of the compound was cultivated and analyzed by diffraction single-crystal method. The influence of the compound in which [Pb(H2O)6][ATZ]·H2O was used as combustion catalyst on the decomposition temperature of potassium nitrate was studied by TG–DSC. The result proved that [Pb(H2O)6][ATZ]·H2O can effectively reduce the decomposition temperature. In other words, [Pb(H2O)6][ATZ]·H2O can reduce the decomposition temperature of potassium nitrate, so the addition of [Pb(H2O)6][ATZ]·H2O can make potassium nitrate better to be used in the fields of initiating explosive device and fire engineering.

KW - Decomposition temperature

KW - Potassium nitrate

KW - Single-crystal lattice

KW - [Pb(HO)][ATZ]·HO

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U2 - 10.1007/s10973-019-08864-8

DO - 10.1007/s10973-019-08864-8

M3 - Article

AN - SCOPUS:85082300396

SN - 1388-6150

VL - 140

SP - 373

EP - 379

JO - Journal of Thermal Analysis and Calorimetry

JF - Journal of Thermal Analysis and Calorimetry

IS - 1

ER -

Synthesis of [Pb(H2O)6][ATZ]·H2O and its impact on potassium nitrate decomposition temperature

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Synthesis of [Pb(H₂O)₆][ATZ]·H₂O and its impact on potassium nitrate decomposition temperature