Preparation and molecular structure of [Pb2(TNR)(NO 3)2(H2O)]

Tong Lai Zhang*, Yong Ming Yang, Jian Guo Zhang, Bing Shao, Li Yang, Kai Bei Yu

*此作品的通讯作者

科研成果: 期刊稿件 › 文章 › 同行评审

10 引用 （Scopus）

摘要

[Pb2(TNR)(NO3)2(H2O)] was prepared by reaction of the aqueous solution of lead nitrate and magnesium styphnate. The crystal structure of Pb2(TNR)(NO3) 2(H2O) was determined by single crystal diffraction analysis. The crystal is triclinic, space group P1 with crystal parameters a = 0.7279(2) nm, b = 1.0698(2) nm, c = 1.0738(2) nm; α = 86. 82(1)°, β = 89.52(2)°, γ = 83.50(2)°; V = 0.8295(3) nm3, Z = 2, Dc = 3.201g · cm-3, F(000) = 716. The final R value is 0.0358. In the crystal structure, one lead ion was represented by nine coordination geometry; the other was showed as ten coordination geometry.

源语言英语
页（从-至）305-308
页数4
期刊Chinese Journal of Inorganic Chemistry
卷18
期3
出版状态已出版 - 2002

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引用此

Zhang, T. L., Yang, Y. M., Zhang, J. G., Shao, B., Yang, L., & Yu, K. B. (2002). Preparation and molecular structure of [Pb2(TNR)(NO 3)2(H2O)]. Chinese Journal of Inorganic Chemistry, 18(3), 305-308.