Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography

Ai Qin Luo; Ai Jun Hou; Rong Ji Dai; Jian Wei Hao; Li Wen Liu

Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography

Ai Qin Luo^*, Ai Jun Hou, Rong Ji Dai, Jian Wei Hao, Li Wen Liu

^*此作品的通讯作者

生命学院

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摘要

Heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase was prepared and separately characterized by IR, XPS and Molisch color reaction. Chromatographic performance of the bonded silica stationary phase was investigated using four kinds of standard samples (uracil, phenol, N,N-dimethylbenzenamine, and toluene) as column efficiency testing materials. At the same time, the separation performance of the stationary phase for separating isomers and two kinds of enantiomers was investigated. The results suggest that some isomers and enantiomers get relative good separation on the stationary phase.

源语言	英语
页（从-至）	745-748
页数	4
期刊	Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology
卷	25
期	8
出版状态	已出版 - 8月 2005

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@article{3cb0a29a24a847f5b74c58a46d550484,

title = "Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography",

abstract = "Heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase was prepared and separately characterized by IR, XPS and Molisch color reaction. Chromatographic performance of the bonded silica stationary phase was investigated using four kinds of standard samples (uracil, phenol, N,N-dimethylbenzenamine, and toluene) as column efficiency testing materials. At the same time, the separation performance of the stationary phase for separating isomers and two kinds of enantiomers was investigated. The results suggest that some isomers and enantiomers get relative good separation on the stationary phase.",

keywords = "Bonded silica, Chiral stationary phase, Heptakis (2,6-di-O-butyl)-β-cyclodextrin, High performance liquid chromatography",

author = "Luo, {Ai Qin} and Hou, {Ai Jun} and Dai, {Rong Ji} and Hao, {Jian Wei} and Liu, {Li Wen}",

year = "2005",

month = aug,

language = "English",

volume = "25",

pages = "745--748",

journal = "Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology",

issn = "1001-0645",

publisher = "Beijing Institute of Technology",

number = "8",

}

Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography. / Luo, Ai Qin; Hou, Ai Jun; Dai, Rong Ji 等.
在: Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology, 卷 25, 号码 8, 08.2005, 页码 745-748.

科研成果: 期刊稿件 › 文章 › 同行评审

TY - JOUR

T1 - Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography

AU - Luo, Ai Qin

AU - Hou, Ai Jun

AU - Dai, Rong Ji

AU - Hao, Jian Wei

AU - Liu, Li Wen

PY - 2005/8

Y1 - 2005/8

N2 - Heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase was prepared and separately characterized by IR, XPS and Molisch color reaction. Chromatographic performance of the bonded silica stationary phase was investigated using four kinds of standard samples (uracil, phenol, N,N-dimethylbenzenamine, and toluene) as column efficiency testing materials. At the same time, the separation performance of the stationary phase for separating isomers and two kinds of enantiomers was investigated. The results suggest that some isomers and enantiomers get relative good separation on the stationary phase.

AB - Heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase was prepared and separately characterized by IR, XPS and Molisch color reaction. Chromatographic performance of the bonded silica stationary phase was investigated using four kinds of standard samples (uracil, phenol, N,N-dimethylbenzenamine, and toluene) as column efficiency testing materials. At the same time, the separation performance of the stationary phase for separating isomers and two kinds of enantiomers was investigated. The results suggest that some isomers and enantiomers get relative good separation on the stationary phase.

KW - Bonded silica

KW - Chiral stationary phase

KW - Heptakis (2,6-di-O-butyl)-β-cyclodextrin

KW - High performance liquid chromatography

UR - http://www.scopus.com/inward/record.url?scp=26644433194&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:26644433194

SN - 1001-0645

VL - 25

SP - 745

EP - 748

JO - Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology

JF - Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology

IS - 8

ER -

Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography

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