Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography

Ai Qin Luo; Ai Jun Hou; Rong Ji Dai; Jian Wei Hao; Li Wen Liu

Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography

Ai Qin Luo^*, Ai Jun Hou, Rong Ji Dai, Jian Wei Hao, Li Wen Liu

^*Corresponding author for this work

School of Life Science

Research output: Contribution to journal › Article › peer-review

Abstract

Heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase was prepared and separately characterized by IR, XPS and Molisch color reaction. Chromatographic performance of the bonded silica stationary phase was investigated using four kinds of standard samples (uracil, phenol, N,N-dimethylbenzenamine, and toluene) as column efficiency testing materials. At the same time, the separation performance of the stationary phase for separating isomers and two kinds of enantiomers was investigated. The results suggest that some isomers and enantiomers get relative good separation on the stationary phase.

Original language	English
Pages (from-to)	745-748
Number of pages	4
Journal	Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology
Volume	25
Issue number	8
Publication status	Published - Aug 2005

Keywords

Bonded silica
Chiral stationary phase
Heptakis (2,6-di-O-butyl)-β-cyclodextrin
High performance liquid chromatography

Cite this

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title = "Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography",

abstract = "Heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase was prepared and separately characterized by IR, XPS and Molisch color reaction. Chromatographic performance of the bonded silica stationary phase was investigated using four kinds of standard samples (uracil, phenol, N,N-dimethylbenzenamine, and toluene) as column efficiency testing materials. At the same time, the separation performance of the stationary phase for separating isomers and two kinds of enantiomers was investigated. The results suggest that some isomers and enantiomers get relative good separation on the stationary phase.",

keywords = "Bonded silica, Chiral stationary phase, Heptakis (2,6-di-O-butyl)-β-cyclodextrin, High performance liquid chromatography",

author = "Luo, {Ai Qin} and Hou, {Ai Jun} and Dai, {Rong Ji} and Hao, {Jian Wei} and Liu, {Li Wen}",

year = "2005",

month = aug,

language = "English",

volume = "25",

pages = "745--748",

journal = "Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology",

issn = "1001-0645",

publisher = "Beijing Institute of Technology",

number = "8",

}

Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography. / Luo, Ai Qin; Hou, Ai Jun; Dai, Rong Ji et al.
In: Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology, Vol. 25, No. 8, 08.2005, p. 745-748.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography

AU - Luo, Ai Qin

AU - Hou, Ai Jun

AU - Dai, Rong Ji

AU - Hao, Jian Wei

AU - Liu, Li Wen

PY - 2005/8

Y1 - 2005/8

N2 - Heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase was prepared and separately characterized by IR, XPS and Molisch color reaction. Chromatographic performance of the bonded silica stationary phase was investigated using four kinds of standard samples (uracil, phenol, N,N-dimethylbenzenamine, and toluene) as column efficiency testing materials. At the same time, the separation performance of the stationary phase for separating isomers and two kinds of enantiomers was investigated. The results suggest that some isomers and enantiomers get relative good separation on the stationary phase.

AB - Heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase was prepared and separately characterized by IR, XPS and Molisch color reaction. Chromatographic performance of the bonded silica stationary phase was investigated using four kinds of standard samples (uracil, phenol, N,N-dimethylbenzenamine, and toluene) as column efficiency testing materials. At the same time, the separation performance of the stationary phase for separating isomers and two kinds of enantiomers was investigated. The results suggest that some isomers and enantiomers get relative good separation on the stationary phase.

KW - Bonded silica

KW - Chiral stationary phase

KW - Heptakis (2,6-di-O-butyl)-β-cyclodextrin

KW - High performance liquid chromatography

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M3 - Article

AN - SCOPUS:26644433194

SN - 1001-0645

VL - 25

SP - 745

EP - 748

JO - Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology

JF - Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology

IS - 8

ER -

Preparation and investigation of the chromatographic performance of heptakis (2,6-di-O-butyl)-β-cyclodextrin bonded silica stationary phase for high performance liquid chromatography

Abstract

Keywords

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