摘要
A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag3SbS3 and Cu3SbS3 from AgNO3 and Cu(NO3)2 and SbCl3 with thiourea at 197°C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.
源语言 | 英语 |
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页(从-至) | 509-513 |
页数 | 5 |
期刊 | Materials Research Bulletin |
卷 | 38 |
期 | 3 |
DOI | |
出版状态 | 已出版 - 20 2月 2003 |
已对外发布 | 是 |