Polyol mediated synthesis of nanocrystalline M3SbS3 (M = Ag, Cu)

Di Chen, Guozhen Shen, Kaibin Tang, Xuan Jiang, Liying Huang, Yin Jin, Yitai Qian

科研成果: 期刊稿件文章同行评审

12 引用 (Scopus)

摘要

A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag3SbS3 and Cu3SbS3 from AgNO3 and Cu(NO3)2 and SbCl3 with thiourea at 197°C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.

源语言英语
页(从-至)509-513
页数5
期刊Materials Research Bulletin
38
3
DOI
出版状态已出版 - 20 2月 2003
已对外发布

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