Polyol mediated synthesis of nanocrystalline M3SbS3 (M = Ag, Cu)

Di Chen; Guozhen Shen; Kaibin Tang; Xuan Jiang; Liying Huang; Yin Jin; Yitai Qian

doi:10.1016/S0025-5408(02)01054-1

Polyol mediated synthesis of nanocrystalline M₃SbS₃ (M = Ag, Cu)

Di Chen, Guozhen Shen, Kaibin Tang, Xuan Jiang, Liying Huang, Yin Jin, Yitai Qian

University of Science and Technology of China

Research output: Contribution to journal › Article › peer-review

12 Citations (Scopus)

Abstract

A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag₃SbS₃ and Cu₃SbS₃ from AgNO₃ and Cu(NO₃)₂ and SbCl₃ with thiourea at 197°C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.

Original language	English
Pages (from-to)	509-513
Number of pages	5
Journal	Materials Research Bulletin
Volume	38
Issue number	3
DOIs	https://doi.org/10.1016/S0025-5408(02)01054-1
Publication status	Published - 20 Feb 2003
Externally published	Yes

Keywords

Chemical synthesis
Electron microscopy
Nanostructures

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10.1016/S0025-5408(02)01054-1

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abstract = "A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag3SbS3 and Cu3SbS3 from AgNO3 and Cu(NO3)2 and SbCl3 with thiourea at 197°C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.",

keywords = "Chemical synthesis, Electron microscopy, Nanostructures",

author = "Di Chen and Guozhen Shen and Kaibin Tang and Xuan Jiang and Liying Huang and Yin Jin and Yitai Qian",

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T1 - Polyol mediated synthesis of nanocrystalline M3SbS3 (M = Ag, Cu)

AU - Chen, Di

AU - Shen, Guozhen

AU - Tang, Kaibin

AU - Jiang, Xuan

AU - Huang, Liying

AU - Jin, Yin

AU - Qian, Yitai

PY - 2003/2/20

Y1 - 2003/2/20

N2 - A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag3SbS3 and Cu3SbS3 from AgNO3 and Cu(NO3)2 and SbCl3 with thiourea at 197°C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.

AB - A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag3SbS3 and Cu3SbS3 from AgNO3 and Cu(NO3)2 and SbCl3 with thiourea at 197°C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.

KW - Chemical synthesis

KW - Electron microscopy

KW - Nanostructures

UR - http://www.scopus.com/inward/record.url?scp=0037456511&partnerID=8YFLogxK

U2 - 10.1016/S0025-5408(02)01054-1

DO - 10.1016/S0025-5408(02)01054-1

M3 - Article

AN - SCOPUS:0037456511

SN - 0025-5408

VL - 38

SP - 509

EP - 513

JO - Materials Research Bulletin

JF - Materials Research Bulletin

IS - 3

ER -

Polyol mediated synthesis of nanocrystalline M₃SbS₃ (M = Ag, Cu)

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Keywords

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