TY - JOUR
T1 - Synthesis and crystal structure of bis(1,3-diisopropyl-4,5-dimethylimidazolium) hexatungstate
AU - Ma, Xiao Li
AU - Sun, Shuai
N1 - Publisher Copyright:
©Copyright Protection
PY - 2014/6/1
Y1 - 2014/6/1
N2 - The title compound bis (1,3-diisopropyl-4,5-dimethylimidazolium) hexatungstate, [C11H21N2]2 [W6O19], was synthesized and characterized by single-crystal X-ray diffraction, IR and elemental analysis. It crystallizes in the monoclinic system, space group P21/n with a=1.112 84(14), b=1.283 84(17), c=1.293 28(17) nm, β=96.410(2)°, V=1.8362(4) nm3, C22H42N4O19W6, Mr=1769.70, Dc=3.201 g/cm3, F(000)=1596, Z=2, μ(MoKα)=18.797 mm-1, the final R=0.0313, wR=0.0598 for observed reflections (I>2σ(I)).
AB - The title compound bis (1,3-diisopropyl-4,5-dimethylimidazolium) hexatungstate, [C11H21N2]2 [W6O19], was synthesized and characterized by single-crystal X-ray diffraction, IR and elemental analysis. It crystallizes in the monoclinic system, space group P21/n with a=1.112 84(14), b=1.283 84(17), c=1.293 28(17) nm, β=96.410(2)°, V=1.8362(4) nm3, C22H42N4O19W6, Mr=1769.70, Dc=3.201 g/cm3, F(000)=1596, Z=2, μ(MoKα)=18.797 mm-1, the final R=0.0313, wR=0.0598 for observed reflections (I>2σ(I)).
KW - Crystal structure
KW - Hexatungstate
KW - N-heterocyclic carbenes
UR - http://www.scopus.com/inward/record.url?scp=84907865190&partnerID=8YFLogxK
M3 - Article
AN - SCOPUS:84907865190
SN - 1004-0579
VL - 23
SP - 265
EP - 269
JO - Journal of Beijing Institute of Technology (English Edition)
JF - Journal of Beijing Institute of Technology (English Edition)
IS - 2
ER -