Preparation and characterization of β-BaB2O4 nanoparticles via coprecipitation

You Fu Zhou; Mao Chun Hong; Yan Qing Xu; Bai Quan Chen; Chang Zhang Chen; Yuan Sheng Wang

doi:10.1016/j.jcrysgro.2004.11.397

Preparation and characterization of β-BaB₂O₄ nanoparticles via coprecipitation

You Fu Zhou, Mao Chun Hong^*, Yan Qing Xu, Bai Quan Chen, Chang Zhang Chen, Yuan Sheng Wang

^*Corresponding author for this work

CAS - Fujian Institute of Research on the Structure of Matter

Research output: Contribution to journal › Article › peer-review

19 Citations (Scopus)

Abstract

β-BaB₂O₄ (β-BBO) nanoparticles have been prepared via coprecipitation using different bases (ammonium hydrogon carbonate, dimethylamine and triethylamine) as precipitants. The precursors and the resulting nanoparticles were characterized by chemical analysis, IR, XRD and TEM. Triethylamine is found to be an optimal precipitant, where the precursor can crystallize into pure β-BBO nanoparticles after annealing at 700 °C for 3 h. TEM analysis reveals that average grain size is ca. 40 nm.

Original language	English
Pages (from-to)	478-484
Number of pages	7
Journal	Journal of Crystal Growth
Volume	276
Issue number	3-4
DOIs	https://doi.org/10.1016/j.jcrysgro.2004.11.397
Publication status	Published - 1 Apr 2005
Externally published	Yes

Keywords

A1. Crystal morphology
A1. X-ray diffraction
B1. Borates
B1. Nanomaterials
B2. Nonlinear optic materials

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10.1016/j.jcrysgro.2004.11.397

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title = "Preparation and characterization of β-BaB2O4 nanoparticles via coprecipitation",

abstract = "β-BaB2O4 (β-BBO) nanoparticles have been prepared via coprecipitation using different bases (ammonium hydrogon carbonate, dimethylamine and triethylamine) as precipitants. The precursors and the resulting nanoparticles were characterized by chemical analysis, IR, XRD and TEM. Triethylamine is found to be an optimal precipitant, where the precursor can crystallize into pure β-BBO nanoparticles after annealing at 700 °C for 3 h. TEM analysis reveals that average grain size is ca. 40 nm.",

keywords = "A1. Crystal morphology, A1. X-ray diffraction, B1. Borates, B1. Nanomaterials, B2. Nonlinear optic materials",

author = "Zhou, {You Fu} and Hong, {Mao Chun} and Xu, {Yan Qing} and Chen, {Bai Quan} and Chen, {Chang Zhang} and Wang, {Yuan Sheng}",

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language = "English",

volume = "276",

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T1 - Preparation and characterization of β-BaB2O4 nanoparticles via coprecipitation

AU - Zhou, You Fu

AU - Hong, Mao Chun

AU - Xu, Yan Qing

AU - Chen, Bai Quan

AU - Chen, Chang Zhang

AU - Wang, Yuan Sheng

PY - 2005/4/1

Y1 - 2005/4/1

N2 - β-BaB2O4 (β-BBO) nanoparticles have been prepared via coprecipitation using different bases (ammonium hydrogon carbonate, dimethylamine and triethylamine) as precipitants. The precursors and the resulting nanoparticles were characterized by chemical analysis, IR, XRD and TEM. Triethylamine is found to be an optimal precipitant, where the precursor can crystallize into pure β-BBO nanoparticles after annealing at 700 °C for 3 h. TEM analysis reveals that average grain size is ca. 40 nm.

AB - β-BaB2O4 (β-BBO) nanoparticles have been prepared via coprecipitation using different bases (ammonium hydrogon carbonate, dimethylamine and triethylamine) as precipitants. The precursors and the resulting nanoparticles were characterized by chemical analysis, IR, XRD and TEM. Triethylamine is found to be an optimal precipitant, where the precursor can crystallize into pure β-BBO nanoparticles after annealing at 700 °C for 3 h. TEM analysis reveals that average grain size is ca. 40 nm.

KW - A1. Crystal morphology

KW - A1. X-ray diffraction

KW - B1. Borates

KW - B1. Nanomaterials

KW - B2. Nonlinear optic materials

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DO - 10.1016/j.jcrysgro.2004.11.397

M3 - Article

AN - SCOPUS:15344343590

SN - 0022-0248

VL - 276

SP - 478

EP - 484

JO - Journal of Crystal Growth

JF - Journal of Crystal Growth

IS - 3-4

ER -

Preparation and characterization of β-BaB₂O₄ nanoparticles via coprecipitation

Abstract

Keywords

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