Preparation and characterization of β-BaB2O4 nanoparticles via coprecipitation

You Fu Zhou; Mao Chun Hong; Yan Qing Xu; Bai Quan Chen; Chang Zhang Chen; Yuan Sheng Wang

doi:10.1016/j.jcrysgro.2004.11.397

Preparation and characterization of β-BaB₂O₄ nanoparticles via coprecipitation

You Fu Zhou, Mao Chun Hong^*, Yan Qing Xu, Bai Quan Chen, Chang Zhang Chen, Yuan Sheng Wang

^*此作品的通讯作者

CAS - Fujian Institute of Research on the Structure of Matter

科研成果: 期刊稿件 › 文章 › 同行评审

19 引用（Scopus）

摘要

β-BaB₂O₄ (β-BBO) nanoparticles have been prepared via coprecipitation using different bases (ammonium hydrogon carbonate, dimethylamine and triethylamine) as precipitants. The precursors and the resulting nanoparticles were characterized by chemical analysis, IR, XRD and TEM. Triethylamine is found to be an optimal precipitant, where the precursor can crystallize into pure β-BBO nanoparticles after annealing at 700 °C for 3 h. TEM analysis reveals that average grain size is ca. 40 nm.

源语言	英语
页（从-至）	478-484
页数	7
期刊	Journal of Crystal Growth
卷	276
期	3-4
DOI	https://doi.org/10.1016/j.jcrysgro.2004.11.397
出版状态	已出版 - 1 4月 2005
已对外发布	是

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title = "Preparation and characterization of β-BaB2O4 nanoparticles via coprecipitation",

abstract = "β-BaB2O4 (β-BBO) nanoparticles have been prepared via coprecipitation using different bases (ammonium hydrogon carbonate, dimethylamine and triethylamine) as precipitants. The precursors and the resulting nanoparticles were characterized by chemical analysis, IR, XRD and TEM. Triethylamine is found to be an optimal precipitant, where the precursor can crystallize into pure β-BBO nanoparticles after annealing at 700 °C for 3 h. TEM analysis reveals that average grain size is ca. 40 nm.",

keywords = "A1. Crystal morphology, A1. X-ray diffraction, B1. Borates, B1. Nanomaterials, B2. Nonlinear optic materials",

author = "Zhou, {You Fu} and Hong, {Mao Chun} and Xu, {Yan Qing} and Chen, {Bai Quan} and Chen, {Chang Zhang} and Wang, {Yuan Sheng}",

year = "2005",

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doi = "10.1016/j.jcrysgro.2004.11.397",

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T1 - Preparation and characterization of β-BaB2O4 nanoparticles via coprecipitation

AU - Zhou, You Fu

AU - Hong, Mao Chun

AU - Xu, Yan Qing

AU - Chen, Bai Quan

AU - Chen, Chang Zhang

AU - Wang, Yuan Sheng

PY - 2005/4/1

Y1 - 2005/4/1

N2 - β-BaB2O4 (β-BBO) nanoparticles have been prepared via coprecipitation using different bases (ammonium hydrogon carbonate, dimethylamine and triethylamine) as precipitants. The precursors and the resulting nanoparticles were characterized by chemical analysis, IR, XRD and TEM. Triethylamine is found to be an optimal precipitant, where the precursor can crystallize into pure β-BBO nanoparticles after annealing at 700 °C for 3 h. TEM analysis reveals that average grain size is ca. 40 nm.

AB - β-BaB2O4 (β-BBO) nanoparticles have been prepared via coprecipitation using different bases (ammonium hydrogon carbonate, dimethylamine and triethylamine) as precipitants. The precursors and the resulting nanoparticles were characterized by chemical analysis, IR, XRD and TEM. Triethylamine is found to be an optimal precipitant, where the precursor can crystallize into pure β-BBO nanoparticles after annealing at 700 °C for 3 h. TEM analysis reveals that average grain size is ca. 40 nm.

KW - A1. Crystal morphology

KW - A1. X-ray diffraction

KW - B1. Borates

KW - B1. Nanomaterials

KW - B2. Nonlinear optic materials

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SN - 0022-0248

VL - 276

SP - 478

EP - 484

JO - Journal of Crystal Growth

JF - Journal of Crystal Growth

IS - 3-4

ER -

Preparation and characterization of β-BaB2O4 nanoparticles via coprecipitation

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Preparation and characterization of β-BaB₂O₄ nanoparticles via coprecipitation