TY - JOUR
T1 - Crystal structure of 2-phenyl-9-hydrazino-1,10-phenanthroline
AU - Yang, Yue
AU - Yang, Peiju
AU - Zhang, Cui
AU - Wu, Biao
PY - 2008
Y1 - 2008
N2 - The title compound, 2-phenyl-9-hydrazino-1,10-phenanthroline, crystallizes in the monoclinic space group P21/c with the following unit-cell parameters: a = 11.7738(3)Å, b = 20.9998(6)Å, c = 12.4546(4)Å, β = 106.750(1)° and V = 2948.71(15)Å3. The crystal structure was solved with a final R = 0.0612 using 6260 independent reflections; it contains two independent molecules in an asymmetric unit, which are joined into a dimer by hydrogen bonds between a phenanthroline N atom and the NH donor of the hydrazine substituent. 2008
AB - The title compound, 2-phenyl-9-hydrazino-1,10-phenanthroline, crystallizes in the monoclinic space group P21/c with the following unit-cell parameters: a = 11.7738(3)Å, b = 20.9998(6)Å, c = 12.4546(4)Å, β = 106.750(1)° and V = 2948.71(15)Å3. The crystal structure was solved with a final R = 0.0612 using 6260 independent reflections; it contains two independent molecules in an asymmetric unit, which are joined into a dimer by hydrogen bonds between a phenanthroline N atom and the NH donor of the hydrazine substituent. 2008
UR - http://www.scopus.com/inward/record.url?scp=58149473773&partnerID=8YFLogxK
U2 - 10.2116/analscix.24.x97
DO - 10.2116/analscix.24.x97
M3 - Comment/debate
AN - SCOPUS:58149473773
SN - 1348-2238
VL - 24
SP - x97-x98
JO - Analytical Sciences: X-ray Structure Analysis Online
JF - Analytical Sciences: X-ray Structure Analysis Online
IS - 5
ER -