A new method to synthesize 3, 3'-diamino-4, 4'-azoxyfurazan (DAOAF)

Min Jie Wu; Shu Sen Chen; Shao Hua Jin; Li Jie Li

doi:10.3969/j.issn.1006-9941.2013.02.024

A new method to synthesize 3, 3'-diamino-4, 4'-azoxyfurazan (DAOAF)

Min Jie Wu^*, Shu Sen Chen, Shao Hua Jin, Li Jie Li

^*Corresponding author for this work

Beijing Institute of Technology

Research output: Contribution to journal › Article › peer-review

5 Citations (Scopus)

Abstract

A new method to synthesize 3, 3'-diamino-4, 4'-azoxyfurazan (DAOAF) which used 3, 4-diaminofurazan as raw material and 3-amino-4-formylaminofurazan or 3, 4-diformylaminofurazan as intermediate was introduced. 3-amino-4-formylaminofurazan or 3, 4-diformylaminofurazan was oxygenating by 30% H₂O₂ in solvent of 1, 4-dioxane. After refluxing for 4 h, DAOAF was obtainded with yield 97% or 89%. The product was characterized by ¹H NMR, ¹³C NMR, IR and EI.

Original language	English
Pages (from-to)	273-275
Number of pages	3
Journal	Hanneng Cailiao/Chinese Journal of Energetic Materials
Volume	21
Issue number	2
DOIs	https://doi.org/10.3969/j.issn.1006-9941.2013.02.024
Publication status	Published - Apr 2013

Keywords

3'-diamino-4, 4'-azoxyfurazan
3, 4-diaminofurazan
3-amino-4-formylaminofurazan
Organic chemistry
Synthesis

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Wu, M. J., Chen, S. S., Jin, S. H., & Li, L. J. (2013). A new method to synthesize 3, 3'-diamino-4, 4'-azoxyfurazan (DAOAF). Hanneng Cailiao/Chinese Journal of Energetic Materials, 21(2), 273-275. https://doi.org/10.3969/j.issn.1006-9941.2013.02.024

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AU - Li, Li Jie

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KW - 3-amino-4-formylaminofurazan

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A new method to synthesize 3, 3'-diamino-4, 4'-azoxyfurazan (DAOAF)

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Keywords

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