摘要
The title compound bis (1,3-diisopropyl-4,5-dimethylimidazolium) hexatungstate, [C11H21N2]2 [W6O19], was synthesized and characterized by single-crystal X-ray diffraction, IR and elemental analysis. It crystallizes in the monoclinic system, space group P21/n with a=1.112 84(14), b=1.283 84(17), c=1.293 28(17) nm, β=96.410(2)°, V=1.8362(4) nm3, C22H42N4O19W6, Mr=1769.70, Dc=3.201 g/cm3, F(000)=1596, Z=2, μ(MoKα)=18.797 mm-1, the final R=0.0313, wR=0.0598 for observed reflections (I>2σ(I)).
源语言 | 英语 |
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页(从-至) | 265-269 |
页数 | 5 |
期刊 | Journal of Beijing Institute of Technology (English Edition) |
卷 | 23 |
期 | 2 |
出版状态 | 已出版 - 1 6月 2014 |
指纹
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Ma, X. L., & Sun, S. (2014). Synthesis and crystal structure of bis(1,3-diisopropyl-4,5-dimethylimidazolium) hexatungstate. Journal of Beijing Institute of Technology (English Edition), 23(2), 265-269.