摘要
Three novel aluminum-containing tin(IV) heterobimetallic sulfides are reported. The reaction of [LAl(SLi)2(THF)2]2 (1) [L = HC(CMeNAr)2, Ar = 2,6-iPr2C6H 3] with Ph2SnCl2, Me2SnCl 2, and SnCl4 in THF respectively afforded LAl(μ-S) 2SnPh2 (2), LAl(μ-S)2SnMe2 (3), and LAl(μ-S)2Sn(μ-S)2AIL (4) in moderate yields. Compounds 2, 3, and 4 were characterized by elemental analysis, NMR, electron-impact mass spectrometry, and single-crystal X-ray structural analysis.
源语言 | 英语 |
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页(从-至) | 3312-3315 |
页数 | 4 |
期刊 | Inorganic Chemistry |
卷 | 45 |
期 | 8 |
DOI | |
出版状态 | 已出版 - 17 4月 2006 |
已对外发布 | 是 |
指纹
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Yang, Z., Ma, X., Jancik, V., Zhang, Z., Roesky, H. W., Magull, J., Noltemeyer, M., Schmidt, H. G., Cea-Olivares, R., & Toscano, R. A. (2006). Synthesis and characterization of aluminum-containing tin(IV) heterobimetallic sulfides. Inorganic Chemistry, 45(8), 3312-3315. https://doi.org/10.1021/ic052139m