Preparation and characterization of layered zirconium phosphates based on water-in-oil microemulsion

Kang Jian Tang; Yang Liu; Zhi Lei Yin; Xue Jing Cao; Ji Hong Yu; Ru Ren Xu

Preparation and characterization of layered zirconium phosphates based on water-in-oil microemulsion

Kang Jian Tang^*, Yang Liu, Zhi Lei Yin, Xue Jing Cao, Ji Hong Yu, Ru Ren Xu

^*此作品的通讯作者

Jilin University

科研成果: 期刊稿件 › 文章 › 同行评审

2 引用（Scopus）

摘要

Layered zirconium phosphates[Zr(HPO₄)₂ · H₂O, (H₃O)⁺Zr₂ (PO₄)₃ and Zr(HPO₄)₈ · H₂O] were synthesized in water/oil(W/O) microemulsion system containing heptane, CTAB/butanol and water. X-ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM) were utilized to characterize the structure, morphology and size. It was found that the preparation of zirconium phosphate in W/O microemulsion could control structure based on the microemulsion composition (i. e. three layered zirconium phosphates obtained with different ratio of water and oil) and morphology based on the reacted conditions (i. e. the size and morphology of α-zirconium phosphate can be controlled with different reacted time and temperature in microemulsion). We believe that the simple synthetic method based on microemulsion would benefit the controllable synthesis of zirconium phosphates greatly.

源语言	英语
页（从-至）	6-9
页数	4
期刊	Kao Teng Hsueh Hsiao Hua Heush Hsueh Pao/ Chemical Journal of Chinese Universities
卷	28
期	1
出版状态	已出版 - 1月 2007
已对外发布	是

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@article{aa574e8c53744cfb948c79a1b71aaeed,

title = "Preparation and characterization of layered zirconium phosphates based on water-in-oil microemulsion",

abstract = "Layered zirconium phosphates[Zr(HPO4)2 · H2O, (H3O)+Zr2 (PO4)3 and Zr(HPO4)8 · H2O] were synthesized in water/oil(W/O) microemulsion system containing heptane, CTAB/butanol and water. X-ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM) were utilized to characterize the structure, morphology and size. It was found that the preparation of zirconium phosphate in W/O microemulsion could control structure based on the microemulsion composition (i. e. three layered zirconium phosphates obtained with different ratio of water and oil) and morphology based on the reacted conditions (i. e. the size and morphology of α-zirconium phosphate can be controlled with different reacted time and temperature in microemulsion). We believe that the simple synthetic method based on microemulsion would benefit the controllable synthesis of zirconium phosphates greatly.",

keywords = "Reverse microemulsion, Water in oil microemulsion, Zirconium phosphates",

author = "Tang, {Kang Jian} and Yang Liu and Yin, {Zhi Lei} and Cao, {Xue Jing} and Yu, {Ji Hong} and Xu, {Ru Ren}",

year = "2007",

month = jan,

language = "English",

volume = "28",

pages = "6--9",

journal = "Kao Teng Hsueh Hsiao Hua Heush Hsueh Pao/ Chemical Journal of Chinese Universities",

issn = "0251-0790",

publisher = "Higher Education Press Limited Company",

number = "1",

}

TY - JOUR

T1 - Preparation and characterization of layered zirconium phosphates based on water-in-oil microemulsion

AU - Tang, Kang Jian

AU - Liu, Yang

AU - Yin, Zhi Lei

AU - Cao, Xue Jing

AU - Yu, Ji Hong

AU - Xu, Ru Ren

PY - 2007/1

Y1 - 2007/1

N2 - Layered zirconium phosphates[Zr(HPO4)2 · H2O, (H3O)+Zr2 (PO4)3 and Zr(HPO4)8 · H2O] were synthesized in water/oil(W/O) microemulsion system containing heptane, CTAB/butanol and water. X-ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM) were utilized to characterize the structure, morphology and size. It was found that the preparation of zirconium phosphate in W/O microemulsion could control structure based on the microemulsion composition (i. e. three layered zirconium phosphates obtained with different ratio of water and oil) and morphology based on the reacted conditions (i. e. the size and morphology of α-zirconium phosphate can be controlled with different reacted time and temperature in microemulsion). We believe that the simple synthetic method based on microemulsion would benefit the controllable synthesis of zirconium phosphates greatly.

AB - Layered zirconium phosphates[Zr(HPO4)2 · H2O, (H3O)+Zr2 (PO4)3 and Zr(HPO4)8 · H2O] were synthesized in water/oil(W/O) microemulsion system containing heptane, CTAB/butanol and water. X-ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM) were utilized to characterize the structure, morphology and size. It was found that the preparation of zirconium phosphate in W/O microemulsion could control structure based on the microemulsion composition (i. e. three layered zirconium phosphates obtained with different ratio of water and oil) and morphology based on the reacted conditions (i. e. the size and morphology of α-zirconium phosphate can be controlled with different reacted time and temperature in microemulsion). We believe that the simple synthetic method based on microemulsion would benefit the controllable synthesis of zirconium phosphates greatly.

KW - Reverse microemulsion

KW - Water in oil microemulsion

KW - Zirconium phosphates

UR - http://www.scopus.com/inward/record.url?scp=34247368873&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:34247368873

SN - 0251-0790

VL - 28

SP - 6

EP - 9

JO - Kao Teng Hsueh Hsiao Hua Heush Hsueh Pao/ Chemical Journal of Chinese Universities

JF - Kao Teng Hsueh Hsiao Hua Heush Hsueh Pao/ Chemical Journal of Chinese Universities

IS - 1

ER -

Preparation and characterization of layered zirconium phosphates based on water-in-oil microemulsion

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