Direct synthesis, crystal structures and thermal analyses of the two-dimensional Cu(ntp)2(H2O)4 crystal (ntp=2-nitroterephthalate)

Jin Yu Guo*, Tong Lai Zhang, Jian Guo Zhang, Yan Hong Liu, Kai Bei Yu

*此作品的通讯作者

科研成果: 期刊稿件 › 文章 › 同行评审

3 引用 （Scopus）

摘要

The Cu(ntp)2(H2O)4 coordination compound has been synthesized by direct method and its crystal has been cultured and characterized by X-ray single crystal structural analysis. The crystal is formulated as C16H16CuN2O16 and crystallized in monoclinic system, space group C2/c, with a=2.2665(7) nm, b=0.7068(2) nm, c=1.575 5(4) nm, β=126.42(1)°, V=2.030 8(13) nm 3, Dc=1.818 g·cm3. Based on DSC and TG-DTG analyses, the thermal decomposition mechanism of Cu(ntp) 2(H2O)4 is predicted that it loses its four coordinated water molecules followed by a large weight loss and formation of copper oxide on heating.

源语言英语
页（从-至）995-999
页数5
期刊Chinese Journal of Inorganic Chemistry
卷22
期6
出版状态已出版 - 6月 2006

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Guo, J. Y., Zhang, T. L., Zhang, J. G., Liu, Y. H., & Yu, K. B. (2006). Direct synthesis, crystal structures and thermal analyses of the two-dimensional Cu(ntp)2(H2O)4 crystal (ntp=2-nitroterephthalate). Chinese Journal of Inorganic Chemistry, 22(6), 995-999.