1-(4-Chloro-2-nitrophenyl)-4,4′-bipyridinium triiodide

Yan Qiong Sun; Jie Zhang; Guo Yu Yang

doi:10.1107/S1600536803006007

1-(4-Chloro-2-nitrophenyl)-4,4′-bipyridinium triiodide

Yan Qiong Sun, Jie Zhang^*, Guo Yu Yang

^*此作品的通讯作者

CAS - Fujian Institute of Research on the Structure of Matter

科研成果: 期刊稿件 › 文章 › 同行评审

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摘要

The title compound, C₁₆H₁₁ClN₃O ₂⁺·I₃^-, consists of a bipyridinium cation and a triiodide anion. The two pyridine rings of the cation are not coplanar, with a dihedral angle of 28.83 (4)°. The benzene ring is also twisted out of the mean plane of the adjoining pyridine ring by 64.27 (5)°. The I₃^- anions are slightly bent and asymmetric, with an I-I-I angle of 178.24 (5)° and I-I bond distances of 2.937(2) and 2.957 (2) Å. The packing shows a columnar arrangement, with parallel stacks of bipyridinium and I₃^- ions along the b axis.

源语言	英语
页（从-至）	o542-o544
期刊	Acta Crystallographica Section E: Structure Reports Online
卷	59
期	4
DOI	https://doi.org/10.1107/S1600536803006007
出版状态	已出版 - 4月 2003
已对外发布	是

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Sun, Y. Q., Zhang, J., & Yang, G. Y. (2003). 1-(4-Chloro-2-nitrophenyl)-4,4′-bipyridinium triiodide. Acta Crystallographica Section E: Structure Reports Online, 59(4), o542-o544. https://doi.org/10.1107/S1600536803006007

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title = "1-(4-Chloro-2-nitrophenyl)-4,4′-bipyridinium triiodide",

abstract = "The title compound, C16H11ClN3O 2+·I3-, consists of a bipyridinium cation and a triiodide anion. The two pyridine rings of the cation are not coplanar, with a dihedral angle of 28.83 (4)°. The benzene ring is also twisted out of the mean plane of the adjoining pyridine ring by 64.27 (5)°. The I3- anions are slightly bent and asymmetric, with an I-I-I angle of 178.24 (5)° and I-I bond distances of 2.937(2) and 2.957 (2) {\AA}. The packing shows a columnar arrangement, with parallel stacks of bipyridinium and I3- ions along the b axis.",

author = "Sun, {Yan Qiong} and Jie Zhang and Yang, {Guo Yu}",

year = "2003",

month = apr,

doi = "10.1107/S1600536803006007",

language = "English",

volume = "59",

pages = "o542--o544",

journal = "Acta Crystallographica Section E: Structure Reports Online",

issn = "1600-5368",

publisher = "International Union of Crystallography",

number = "4",

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TY - JOUR

T1 - 1-(4-Chloro-2-nitrophenyl)-4,4′-bipyridinium triiodide

AU - Sun, Yan Qiong

AU - Zhang, Jie

AU - Yang, Guo Yu

PY - 2003/4

Y1 - 2003/4

N2 - The title compound, C16H11ClN3O 2+·I3-, consists of a bipyridinium cation and a triiodide anion. The two pyridine rings of the cation are not coplanar, with a dihedral angle of 28.83 (4)°. The benzene ring is also twisted out of the mean plane of the adjoining pyridine ring by 64.27 (5)°. The I3- anions are slightly bent and asymmetric, with an I-I-I angle of 178.24 (5)° and I-I bond distances of 2.937(2) and 2.957 (2) Å. The packing shows a columnar arrangement, with parallel stacks of bipyridinium and I3- ions along the b axis.

AB - The title compound, C16H11ClN3O 2+·I3-, consists of a bipyridinium cation and a triiodide anion. The two pyridine rings of the cation are not coplanar, with a dihedral angle of 28.83 (4)°. The benzene ring is also twisted out of the mean plane of the adjoining pyridine ring by 64.27 (5)°. The I3- anions are slightly bent and asymmetric, with an I-I-I angle of 178.24 (5)° and I-I bond distances of 2.937(2) and 2.957 (2) Å. The packing shows a columnar arrangement, with parallel stacks of bipyridinium and I3- ions along the b axis.

UR - http://www.scopus.com/inward/record.url?scp=18444390922&partnerID=8YFLogxK

U2 - 10.1107/S1600536803006007

DO - 10.1107/S1600536803006007

M3 - Article

AN - SCOPUS:18444390922

SN - 1600-5368

VL - 59

SP - o542-o544

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 4

ER -

1-(4-Chloro-2-nitrophenyl)-4,4′-bipyridinium triiodide

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