Synthesis and performance of 4, 5-dicyano- 2H-1, 2, 3-triazole

Ying Hao Zhang; Zhi Ming Du; Zhi Yue Han; Qian Yao

doi:10.15918/j.jbit1004-0579.201625.S101

Synthesis and performance of 4, 5-dicyano- 2H-1, 2, 3-triazole

Ying Hao Zhang, Zhi Ming Du, Zhi Yue Han^*, Qian Yao

^*Corresponding author for this work

School of Mechatronical Engineering

Beijing Institute of Technology

Research output: Contribution to journal › Article › peer-review

Abstract

4, 5-Dicyano-2H-1, 2, 3-triazole(DCT) was synthesized with diaminomaleodinitrile as the raw material. The structure of DCT was charactered by IR, ¹H NMR, ¹³C NMR and EA. Its synthesis process was optimized. The thermal stability of DCT was investigated by TG-DSC technique. The kinetic parameters including activation energy and pro-exponential factor were calculated by Kissinger equation. Its hygroscopicity, impact and friction sensitivities were also measured. 4, 5-dicyano-2H-1, 2, 3-triazole has potential application prospect as environmentally friendly gas generant, explosive and solid propellant.

Original language	English
Pages (from-to)	1-5
Number of pages	5
Journal	Journal of Beijing Institute of Technology (English Edition)
Volume	25
DOIs	https://doi.org/10.15918/j.jbit1004-0579.201625.S101
Publication status	Published - 1 May 2016

Keywords

4, 5-dicyano-2H-1, 2, 3-triazole
Performance
Synthesis optimization
Thermal stability

Access to Document

10.15918/j.jbit1004-0579.201625.S101

Cite this

Zhang, Y. H., Du, Z. M., Han, Z. Y., & Yao, Q. (2016). Synthesis and performance of 4, 5-dicyano- 2H-1, 2, 3-triazole. Journal of Beijing Institute of Technology (English Edition), 25, 1-5. https://doi.org/10.15918/j.jbit1004-0579.201625.S101

@article{cdefd9517cdf4ba4955d57ea7816e14c,

title = "Synthesis and performance of 4, 5-dicyano- 2H-1, 2, 3-triazole",

abstract = "4, 5-Dicyano-2H-1, 2, 3-triazole(DCT) was synthesized with diaminomaleodinitrile as the raw material. The structure of DCT was charactered by IR, 1H NMR, 13C NMR and EA. Its synthesis process was optimized. The thermal stability of DCT was investigated by TG-DSC technique. The kinetic parameters including activation energy and pro-exponential factor were calculated by Kissinger equation. Its hygroscopicity, impact and friction sensitivities were also measured. 4, 5-dicyano-2H-1, 2, 3-triazole has potential application prospect as environmentally friendly gas generant, explosive and solid propellant.",

keywords = "4, 5-dicyano-2H-1, 2, 3-triazole, Performance, Synthesis optimization, Thermal stability",

author = "Zhang, {Ying Hao} and Du, {Zhi Ming} and Han, {Zhi Yue} and Qian Yao",

note = "Publisher Copyright: {\textcopyright} 2016 Beijing Institute of Technology.",

year = "2016",

month = may,

day = "1",

doi = "10.15918/j.jbit1004-0579.201625.S101",

language = "English",

volume = "25",

pages = "1--5",

journal = "Journal of Beijing Institute of Technology (English Edition)",

issn = "1004-0579",

publisher = "Beijing Institute of Technology",

}

TY - JOUR

T1 - Synthesis and performance of 4, 5-dicyano- 2H-1, 2, 3-triazole

AU - Zhang, Ying Hao

AU - Du, Zhi Ming

AU - Han, Zhi Yue

AU - Yao, Qian

PY - 2016/5/1

Y1 - 2016/5/1

N2 - 4, 5-Dicyano-2H-1, 2, 3-triazole(DCT) was synthesized with diaminomaleodinitrile as the raw material. The structure of DCT was charactered by IR, 1H NMR, 13C NMR and EA. Its synthesis process was optimized. The thermal stability of DCT was investigated by TG-DSC technique. The kinetic parameters including activation energy and pro-exponential factor were calculated by Kissinger equation. Its hygroscopicity, impact and friction sensitivities were also measured. 4, 5-dicyano-2H-1, 2, 3-triazole has potential application prospect as environmentally friendly gas generant, explosive and solid propellant.

AB - 4, 5-Dicyano-2H-1, 2, 3-triazole(DCT) was synthesized with diaminomaleodinitrile as the raw material. The structure of DCT was charactered by IR, 1H NMR, 13C NMR and EA. Its synthesis process was optimized. The thermal stability of DCT was investigated by TG-DSC technique. The kinetic parameters including activation energy and pro-exponential factor were calculated by Kissinger equation. Its hygroscopicity, impact and friction sensitivities were also measured. 4, 5-dicyano-2H-1, 2, 3-triazole has potential application prospect as environmentally friendly gas generant, explosive and solid propellant.

KW - 4, 5-dicyano-2H-1, 2, 3-triazole

KW - Performance

KW - Synthesis optimization

KW - Thermal stability

UR - http://www.scopus.com/inward/record.url?scp=84973474073&partnerID=8YFLogxK

U2 - 10.15918/j.jbit1004-0579.201625.S101

DO - 10.15918/j.jbit1004-0579.201625.S101

M3 - Article

AN - SCOPUS:84973474073

SN - 1004-0579

VL - 25

SP - 1

EP - 5

JO - Journal of Beijing Institute of Technology (English Edition)

JF - Journal of Beijing Institute of Technology (English Edition)

ER -

Synthesis and performance of 4, 5-dicyano- 2H-1, 2, 3-triazole

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this