Abstract
The title compound, C 21H 21N 3O, was obtained by cyclo-condensation of 3-amino-5-methyl-[1,1′-biphen-yl]-2,4- di-car-bo-nitrile with cyclo-hexa-none. The six-membered 1,3-diaza ring assumes an envelope conformation [with the flap atom displaced by 0.511 (7) Å from the plane through the other ring atoms] and the cyclo-hexane ring displays a chair conformation. The dihedral angle between the aromatic rings is 42.61 (7)°.In the crystal, the mol-ecules form hydrogen-bonded bands along [011].
Original language | English |
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Pages (from-to) | o1672 |
Journal | Acta Crystallographica Section E: Structure Reports Online |
Volume | 67 |
Issue number | 7 |
DOIs | |
Publication status | Published - Jul 2011 |
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Tang, J., Shi, D., Yan, L., Liu, X., & Li, J. (2011). 5′-Methyl-4′-oxo-7′-phenyl-3′,4′-dihydro- 1′H-spiro-[cyclo-hexane-1,2′-quinazoline]-8′-carbonitrile. Acta Crystallographica Section E: Structure Reports Online, 67(7), o1672. https://doi.org/10.1107/S160053681102188X