TY - JOUR
T1 - Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate
AU - Jianguo, Zhang
AU - Tonglai, Zhang
AU - Kaibei, Yu
PY - 2003/4
Y1 - 2003/4
N2 - 4-Amino-1,2,4-triazol-5-one hydrate (ATO·H2O) was prepared and its structure was analyzed by four-circle diffraction measurement. The obtained results show that the crystal belongs to the triclinic crystal system, space group P 1 with crystal parameters a = 6.432(1), b = 6.551(1), c = 6.740(1) Å; α = 68.04(1), β = 82.18(1), γ = 81.90(1)°; V = 259.7(7) Å3; Z = 2; Dc = 1.510g/cm 3; μ = 0.131 mm-1; F(000) = 124. ATO·H 2O was characterized by FT-IR analysis, X-ray diffraction analysis, and single crystal diffraction analysis.
AB - 4-Amino-1,2,4-triazol-5-one hydrate (ATO·H2O) was prepared and its structure was analyzed by four-circle diffraction measurement. The obtained results show that the crystal belongs to the triclinic crystal system, space group P 1 with crystal parameters a = 6.432(1), b = 6.551(1), c = 6.740(1) Å; α = 68.04(1), β = 82.18(1), γ = 81.90(1)°; V = 259.7(7) Å3; Z = 2; Dc = 1.510g/cm 3; μ = 0.131 mm-1; F(000) = 124. ATO·H 2O was characterized by FT-IR analysis, X-ray diffraction analysis, and single crystal diffraction analysis.
KW - 4-amino-1,2,4-triazol-5-one
KW - Crystal structure
KW - Molecular structure
KW - Structure characterization
UR - http://www.scopus.com/inward/record.url?scp=0142091651&partnerID=8YFLogxK
U2 - 10.1023/A:1024709212512
DO - 10.1023/A:1024709212512
M3 - Article
AN - SCOPUS:0142091651
SN - 0009-3122
VL - 39
SP - 461
EP - 466
JO - Chemistry of Heterocyclic Compounds
JF - Chemistry of Heterocyclic Compounds
IS - 4
ER -