Preparation and molecular structure of semicarbazide picric

Li Yang; Tong Lai Zhang; Jian Guo Zhang; Bing Shao; Chang Gen Feng; Kai Bei Yu

Preparation and molecular structure of semicarbazide picric

Li Yang^*, Tong Lai Zhang, Jian Guo Zhang, Bing Shao, Chang Gen Feng, Kai Bei Yu

^*此作品的通讯作者

机电学院

科研成果: 期刊稿件 › 文章 › 同行评审

6 引用（Scopus）

摘要

Abstract; The preparation method and structure analysis results were obtained for the salt made from semicarbazide and picric acid. The molecular structure was characterized by elemental analysis, IR and DSC. Its crystal structure was determined by the single-crystal X-ray diffraction method with a four-circle diffractometer. The results show that the crystal is of triclinic system. Space group is Pi with crystal parameters of a =5. 024(1) Å, 6 = 10.209( I ) Å.'c = 11.551 ( 1 ) Å;a =79.00(1 )°, β = 81. 11 ( 1)°, γ=82.47(1)0;K = 571.42(14)Å³, Z =2, D_C = 1.768 g ·cm^-3, μ =0. 162 mm"', F(000) =312, R₁ = 0.032 4, Rw₂ =0.087 40.

源语言	英语
页（从-至）	75-76
页数	2
期刊	Hanneng Cailiao/Chinese Journal of Energetic Materials
卷	9
期	2
出版状态	已出版 - 2001

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@article{cbe18ce523b640e09675eedd5da9b17f,

title = "Preparation and molecular structure of semicarbazide picric",

abstract = "Abstract; The preparation method and structure analysis results were obtained for the salt made from semicarbazide and picric acid. The molecular structure was characterized by elemental analysis, IR and DSC. Its crystal structure was determined by the single-crystal X-ray diffraction method with a four-circle diffractometer. The results show that the crystal is of triclinic system. Space group is Pi with crystal parameters of a =5. 024(1) {\AA}, 6 = 10.209( I ) {\AA}.'c = 11.551 ( 1 ) {\AA};a =79.00(1 )°, β = 81. 11 ( 1)°, γ=82.47(1)0;K = 571.42(14){\AA}3, Z =2, DC = 1.768 g ·cm-3, μ =0. 162 mm{"}', F(000) =312, R1 = 0.032 4, Rw2 =0.087 40.",

keywords = "Crystal structure, Molecular structure, Preparation, Semicarbazide picric",

author = "Li Yang and Zhang, {Tong Lai} and Zhang, {Jian Guo} and Bing Shao and Feng, {Chang Gen} and Yu, {Kai Bei}",

year = "2001",

language = "English",

volume = "9",

pages = "75--76",

journal = "Hanneng Cailiao/Chinese Journal of Energetic Materials",

issn = "1006-9941",

publisher = "Institute of Chemical Materials, China Academy of Engineering Physics",

number = "2",

}

TY - JOUR

T1 - Preparation and molecular structure of semicarbazide picric

AU - Yang, Li

AU - Zhang, Tong Lai

AU - Zhang, Jian Guo

AU - Shao, Bing

AU - Feng, Chang Gen

AU - Yu, Kai Bei

PY - 2001

Y1 - 2001

N2 - Abstract; The preparation method and structure analysis results were obtained for the salt made from semicarbazide and picric acid. The molecular structure was characterized by elemental analysis, IR and DSC. Its crystal structure was determined by the single-crystal X-ray diffraction method with a four-circle diffractometer. The results show that the crystal is of triclinic system. Space group is Pi with crystal parameters of a =5. 024(1) Å, 6 = 10.209( I ) Å.'c = 11.551 ( 1 ) Å;a =79.00(1 )°, β = 81. 11 ( 1)°, γ=82.47(1)0;K = 571.42(14)Å3, Z =2, DC = 1.768 g ·cm-3, μ =0. 162 mm"', F(000) =312, R1 = 0.032 4, Rw2 =0.087 40.

AB - Abstract; The preparation method and structure analysis results were obtained for the salt made from semicarbazide and picric acid. The molecular structure was characterized by elemental analysis, IR and DSC. Its crystal structure was determined by the single-crystal X-ray diffraction method with a four-circle diffractometer. The results show that the crystal is of triclinic system. Space group is Pi with crystal parameters of a =5. 024(1) Å, 6 = 10.209( I ) Å.'c = 11.551 ( 1 ) Å;a =79.00(1 )°, β = 81. 11 ( 1)°, γ=82.47(1)0;K = 571.42(14)Å3, Z =2, DC = 1.768 g ·cm-3, μ =0. 162 mm"', F(000) =312, R1 = 0.032 4, Rw2 =0.087 40.

KW - Crystal structure

KW - Molecular structure

KW - Preparation

KW - Semicarbazide picric

UR - http://www.scopus.com/inward/record.url?scp=0034932405&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:0034932405

SN - 1006-9941

VL - 9

SP - 75

EP - 76

JO - Hanneng Cailiao/Chinese Journal of Energetic Materials

JF - Hanneng Cailiao/Chinese Journal of Energetic Materials

IS - 2

ER -

Preparation and molecular structure of semicarbazide picric

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