Preparation and molecular structure of {[Ag(ATO)2]ClO4}n

Jian Guo Zhang; Tong Lai Zhang; Zhi Gang Zhang; Kai Bei Yu

Preparation and molecular structure of {[Ag(ATO)₂]ClO₄}_n

Jian Guo Zhang^*, Tong Lai Zhang, Zhi Gang Zhang, Kai Bei Yu

^*此作品的通讯作者

机电学院

科研成果: 期刊稿件 › 文章 › 同行评审

23 引用（Scopus）

摘要

{[Ag(ATO)₂]Cl04}_n was prepared by mixing the aqueous solutions of 4-amino-1,2,4-triazol-5-one and silver perchlorate. The product was characterized by thermal analysis, TG-DTG, element analysis, and IR measurement. The crystal structure of [Ag(ATO)₂]ClO₄ was determined by single crystal diffraction analysis. The crystal is triclinic, space group P1 with crystal parameters of a = 0.7534(1)nm, b = 0.8505(1)nm, c = 1.0257(1)nm; a = 69.47(1)°, β = 72.69(1)°, γ = 86.00(1)°; V = 0.5872(1)nm³, Z = 2, D_c = 2.305g/cm³, F(000) = 400. The final R is 0. 0358. The silver ion represents three coordination geometry with three different nitrogen atoms.

源语言	英语
页（从-至）	533-537
页数	5
期刊	Acta Chimica Sinica
卷	58
期	5
出版状态	已出版 - 2000

其它文件与链接

链接到 Scopus 的出版物

引用此

@article{6a838fd998784d98b48e27fa35b78abf,

title = "Preparation and molecular structure of {[Ag(ATO)2]ClO4}n ",

abstract = "{[Ag(ATO)2]Cl04}n was prepared by mixing the aqueous solutions of 4-amino-1,2,4-triazol-5-one and silver perchlorate. The product was characterized by thermal analysis, TG-DTG, element analysis, and IR measurement. The crystal structure of [Ag(ATO)2]ClO4 was determined by single crystal diffraction analysis. The crystal is triclinic, space group P1 with crystal parameters of a = 0.7534(1)nm, b = 0.8505(1)nm, c = 1.0257(1)nm; a = 69.47(1)°, β = 72.69(1)°, γ = 86.00(1)°; V = 0.5872(1)nm3, Z = 2, Dc = 2.305g/cm3, F(000) = 400. The final R is 0. 0358. The silver ion represents three coordination geometry with three different nitrogen atoms.",

keywords = "4-amino-1,2,4-triazol-5-one (ATO), Crystal structure, Molecular structure, Preparation, Silver complex",

author = "Zhang, {Jian Guo} and Zhang, {Tong Lai} and Zhang, {Zhi Gang} and Yu, {Kai Bei}",

year = "2000",

language = "English",

volume = "58",

pages = "533--537",

journal = "Acta Chimica Sinica",

issn = "0567-7351",

publisher = "Science China Press",

number = "5",

}

TY - JOUR

T1 - Preparation and molecular structure of {[Ag(ATO)2]ClO4}n

AU - Zhang, Jian Guo

AU - Zhang, Tong Lai

AU - Zhang, Zhi Gang

AU - Yu, Kai Bei

PY - 2000

Y1 - 2000

N2 - {[Ag(ATO)2]Cl04}n was prepared by mixing the aqueous solutions of 4-amino-1,2,4-triazol-5-one and silver perchlorate. The product was characterized by thermal analysis, TG-DTG, element analysis, and IR measurement. The crystal structure of [Ag(ATO)2]ClO4 was determined by single crystal diffraction analysis. The crystal is triclinic, space group P1 with crystal parameters of a = 0.7534(1)nm, b = 0.8505(1)nm, c = 1.0257(1)nm; a = 69.47(1)°, β = 72.69(1)°, γ = 86.00(1)°; V = 0.5872(1)nm3, Z = 2, Dc = 2.305g/cm3, F(000) = 400. The final R is 0. 0358. The silver ion represents three coordination geometry with three different nitrogen atoms.

AB - {[Ag(ATO)2]Cl04}n was prepared by mixing the aqueous solutions of 4-amino-1,2,4-triazol-5-one and silver perchlorate. The product was characterized by thermal analysis, TG-DTG, element analysis, and IR measurement. The crystal structure of [Ag(ATO)2]ClO4 was determined by single crystal diffraction analysis. The crystal is triclinic, space group P1 with crystal parameters of a = 0.7534(1)nm, b = 0.8505(1)nm, c = 1.0257(1)nm; a = 69.47(1)°, β = 72.69(1)°, γ = 86.00(1)°; V = 0.5872(1)nm3, Z = 2, Dc = 2.305g/cm3, F(000) = 400. The final R is 0. 0358. The silver ion represents three coordination geometry with three different nitrogen atoms.

KW - 4-amino-1,2,4-triazol-5-one (ATO)

KW - Crystal structure

KW - Molecular structure

KW - Preparation

KW - Silver complex

UR - http://www.scopus.com/inward/record.url?scp=0041779622&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:0041779622

SN - 0567-7351

VL - 58

SP - 533

EP - 537

JO - Acta Chimica Sinica

JF - Acta Chimica Sinica

IS - 5

ER -

Preparation and molecular structure of {[Ag(ATO)2]ClO4}n

摘要

其它文件与链接

指纹

引用此

Preparation and molecular structure of {[Ag(ATO)₂]ClO₄}_n