摘要
[Ag(TO)2]ClO4·H2O was prepared by mixing the aqueous solution of 1,2,4-triazol-5-one(TO) and silver perchlorate. It was characterized by X-ray diffraction, TG-DTG, and IR measurement. The crystal is triclinic, space group P1 with a = 0.533(1) nm, b = 0.938(1) nm, c = 1.220(1) nm; α = 88.02(1)°, β = 79.50(1)°, γ = 82.86(1)°; V = 0.5953(8) nm3, Z = 2, R is 0.0281. The silver atom has a slightly bent linear coordination geometry with two nitrogen atoms.
源语言 | 英语 |
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页(从-至) | 1238 |
页数 | 1 |
期刊 | Acta Chimica Sinica |
卷 | 57 |
期 | 11 |
出版状态 | 已出版 - 11月 1999 |