Preparation and characterization of nano-CNTs/KNO3 composites

Qing Zhong Cui; Qing Jie Jiao; Shuai Liu

doi:10.3969/j.issn.1006-9941.2009.06.011

Preparation and characterization of nano-CNTs/KNO₃ composites

Qing Zhong Cui^*, Qing Jie Jiao, Shuai Liu

^*此作品的通讯作者

机电学院

Beijing Institute of Technology

科研成果: 期刊稿件 › 文章 › 同行评审

3 引用（Scopus）

摘要

The carbon nano-tubes/potassium nitrate (CNTs/KNO₃) composites were prepared by recrystalization and neutralization method respectively. Micro-morphologies and thermal decomposition properties were characterized by scanning electron mitroscope (SEM), X-ray diffraction (XRD), specific surface area (SSA) and differential scanning calorimeter (DSC). The results show that KNO₃ is coated on the surface of CNTs by two methods. SSA of the nano-CNTs/KNO₃ composites by recrystalization decreases about 113.9 m²·g^-1 compared with that of CNTs, while the thermal decomposition temperature is the same as that of KNO₃. SSA of the nano-CNTs/KNO₃ composites prepared by neutralization decreases about 138.7 m²·g^-1 compared with that of CNTs, and the thermal decomposition temperature decreases about 28°C compared with that of KNO₃. Results show that in neutralization, CNTs has catalytic effect on the thermal decomposition of KNO₃.

源语言	英语
页（从-至）	685-688
页数	4
期刊	Hanneng Cailiao/Chinese Journal of Energetic Materials
卷	17
期	6
DOI	https://doi.org/10.3969/j.issn.1006-9941.2009.06.011
出版状态	已出版 - 12月 2009

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Cui, Q. Z., Jiao, Q. J., & Liu, S. (2009). Preparation and characterization of nano-CNTs/KNO₃ composites. Hanneng Cailiao/Chinese Journal of Energetic Materials, 17(6), 685-688. https://doi.org/10.3969/j.issn.1006-9941.2009.06.011

@article{af96308152e345738604ce8dde67a12b,

title = "Preparation and characterization of nano-CNTs/KNO3 composites",

abstract = "The carbon nano-tubes/potassium nitrate (CNTs/KNO3) composites were prepared by recrystalization and neutralization method respectively. Micro-morphologies and thermal decomposition properties were characterized by scanning electron mitroscope (SEM), X-ray diffraction (XRD), specific surface area (SSA) and differential scanning calorimeter (DSC). The results show that KNO3 is coated on the surface of CNTs by two methods. SSA of the nano-CNTs/KNO3 composites by recrystalization decreases about 113.9 m2·g-1 compared with that of CNTs, while the thermal decomposition temperature is the same as that of KNO3. SSA of the nano-CNTs/KNO3 composites prepared by neutralization decreases about 138.7 m2·g-1 compared with that of CNTs, and the thermal decomposition temperature decreases about 28°C compared with that of KNO3. Results show that in neutralization, CNTs has catalytic effect on the thermal decomposition of KNO3.",

keywords = "Carbon nano-tubes (CNTs), KNO, Nano-composite, Physical chemistry, Thermal decomposition",

author = "Cui, {Qing Zhong} and Jiao, {Qing Jie} and Shuai Liu",

year = "2009",

month = dec,

doi = "10.3969/j.issn.1006-9941.2009.06.011",

language = "English",

volume = "17",

pages = "685--688",

journal = "Hanneng Cailiao/Chinese Journal of Energetic Materials",

issn = "1006-9941",

publisher = "Institute of Chemical Materials, China Academy of Engineering Physics",

number = "6",

}

TY - JOUR

T1 - Preparation and characterization of nano-CNTs/KNO3 composites

AU - Cui, Qing Zhong

AU - Jiao, Qing Jie

AU - Liu, Shuai

PY - 2009/12

Y1 - 2009/12

N2 - The carbon nano-tubes/potassium nitrate (CNTs/KNO3) composites were prepared by recrystalization and neutralization method respectively. Micro-morphologies and thermal decomposition properties were characterized by scanning electron mitroscope (SEM), X-ray diffraction (XRD), specific surface area (SSA) and differential scanning calorimeter (DSC). The results show that KNO3 is coated on the surface of CNTs by two methods. SSA of the nano-CNTs/KNO3 composites by recrystalization decreases about 113.9 m2·g-1 compared with that of CNTs, while the thermal decomposition temperature is the same as that of KNO3. SSA of the nano-CNTs/KNO3 composites prepared by neutralization decreases about 138.7 m2·g-1 compared with that of CNTs, and the thermal decomposition temperature decreases about 28°C compared with that of KNO3. Results show that in neutralization, CNTs has catalytic effect on the thermal decomposition of KNO3.

AB - The carbon nano-tubes/potassium nitrate (CNTs/KNO3) composites were prepared by recrystalization and neutralization method respectively. Micro-morphologies and thermal decomposition properties were characterized by scanning electron mitroscope (SEM), X-ray diffraction (XRD), specific surface area (SSA) and differential scanning calorimeter (DSC). The results show that KNO3 is coated on the surface of CNTs by two methods. SSA of the nano-CNTs/KNO3 composites by recrystalization decreases about 113.9 m2·g-1 compared with that of CNTs, while the thermal decomposition temperature is the same as that of KNO3. SSA of the nano-CNTs/KNO3 composites prepared by neutralization decreases about 138.7 m2·g-1 compared with that of CNTs, and the thermal decomposition temperature decreases about 28°C compared with that of KNO3. Results show that in neutralization, CNTs has catalytic effect on the thermal decomposition of KNO3.

KW - Carbon nano-tubes (CNTs)

KW - KNO

KW - Nano-composite

KW - Physical chemistry

KW - Thermal decomposition

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JO - Hanneng Cailiao/Chinese Journal of Energetic Materials

JF - Hanneng Cailiao/Chinese Journal of Energetic Materials

IS - 6

ER -

Preparation and characterization of nano-CNTs/KNO3 composites

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Preparation and characterization of nano-CNTs/KNO₃ composites