TY - JOUR
T1 - Hydrothermal synthesis and structure of a novel hybrid germanium vanadate
T2 - (2,2′-bpy)2(VVO2) 2(H2GeO4)·6H2O
AU - Zheng, Shou Tian
AU - Zhang, Jie
AU - Yang, Guo Yu
PY - 2004/7
Y1 - 2004/7
N2 - A new hybrid germanium vanadate (2,2′-bpy) 2(VVO2)2(H2GeO 4)·6H2O 1 (2,2′-bpy=2,2 ′-bipyridine) was synthesized by hydrothermal method and structurally characterized by single-crystal X-ray diffraction, thermogravimetric analysis (TGA), IR, XRD and elemental analyses. Crystal data for 1: monoclinic, C2/c, a=16.6937(9) Å, b=11.3501(6) Å, c=17.4774(9) Å, β=118.19(2)°, V=2918.7(3) Å3, Z=4. Compound 1 is composed of the first germanium vanadate skeleton covalently attached to 2,2′-bpy ligands.
AB - A new hybrid germanium vanadate (2,2′-bpy) 2(VVO2)2(H2GeO 4)·6H2O 1 (2,2′-bpy=2,2 ′-bipyridine) was synthesized by hydrothermal method and structurally characterized by single-crystal X-ray diffraction, thermogravimetric analysis (TGA), IR, XRD and elemental analyses. Crystal data for 1: monoclinic, C2/c, a=16.6937(9) Å, b=11.3501(6) Å, c=17.4774(9) Å, β=118.19(2)°, V=2918.7(3) Å3, Z=4. Compound 1 is composed of the first germanium vanadate skeleton covalently attached to 2,2′-bpy ligands.
KW - Crystal structure
KW - Germanate
KW - Hydrothermal synthesis
KW - Inorganic-organic hybrid
KW - Vanadate
UR - http://www.scopus.com/inward/record.url?scp=3242738548&partnerID=8YFLogxK
U2 - 10.1016/j.inoche.2004.05.007
DO - 10.1016/j.inoche.2004.05.007
M3 - Article
AN - SCOPUS:3242738548
SN - 1387-7003
VL - 7
SP - 861
EP - 863
JO - Inorganic Chemistry Communications
JF - Inorganic Chemistry Communications
IS - 7
ER -