Growth and characterizations of La2CaB10O19 crystal from the new Li2B4O7−MoO3 flux system with lower volatility and viscosity

Jingcheng Feng; Feidi Fan; Yuwei Chen; Wang Liu; Jun Shen; Guochun Zhang; Heng Tu

doi:10.1016/j.jcrysgro.2021.126383

Growth and characterizations of La₂CaB₁₀O₁₉ crystal from the new Li₂B₄O₇−MoO₃ flux system with lower volatility and viscosity

Jingcheng Feng, Feidi Fan, Yuwei Chen, Wang Liu, Jun Shen, Guochun Zhang^*, Heng Tu

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摘要

A new flux, Li₂B₄O₇ − MoO₃, has been successfully used to grow La₂CaB₁₀O₁₉ (LCB) single crystals by the top seeded solution growth (TSSG) method. The suitable region for LCB crystal growth was investigated by growth experiments, and measurements of volatility and viscosity, which confirmed that the appropriate molar ratios of LCB: Li₂B₄O₇: MoO₃ are 1: 2.3: (1–1.5). The characterizations, including X-ray rocking curve, transmission spectra, optical weak absorption, and laser-induced damage threshold, have been performed on the as-grown crystal, which indicated that the LCB crystal grown from new LCB − Li₂B₄O₇ − MoO₃ system exhibits high optical quality.

源语言	英语
文章编号	126383
期刊	Journal of Crystal Growth
卷	576
DOI	https://doi.org/10.1016/j.jcrysgro.2021.126383
出版状态	已出版 - 15 12月 2021
已对外发布	是

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title = "Growth and characterizations of La2CaB10O19 crystal from the new Li2B4O7−MoO3 flux system with lower volatility and viscosity",

abstract = "A new flux, Li2B4O7 − MoO3, has been successfully used to grow La2CaB10O19 (LCB) single crystals by the top seeded solution growth (TSSG) method. The suitable region for LCB crystal growth was investigated by growth experiments, and measurements of volatility and viscosity, which confirmed that the appropriate molar ratios of LCB: Li2B4O7: MoO3 are 1: 2.3: (1–1.5). The characterizations, including X-ray rocking curve, transmission spectra, optical weak absorption, and laser-induced damage threshold, have been performed on the as-grown crystal, which indicated that the LCB crystal grown from new LCB − Li2B4O7 − MoO3 system exhibits high optical quality.",

keywords = "A1. Characterization, A2. Top seeded solution growth, B1. Lanthanum calcium borates, B2. Nonlinear optical materials",

author = "Jingcheng Feng and Feidi Fan and Yuwei Chen and Wang Liu and Jun Shen and Guochun Zhang and Heng Tu",

note = "Publisher Copyright: {\textcopyright} 2021 Elsevier B.V.",

year = "2021",

month = dec,

day = "15",

doi = "10.1016/j.jcrysgro.2021.126383",

language = "English",

volume = "576",

journal = "Journal of Crystal Growth",

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TY - JOUR

T1 - Growth and characterizations of La2CaB10O19 crystal from the new Li2B4O7−MoO3 flux system with lower volatility and viscosity

AU - Feng, Jingcheng

AU - Fan, Feidi

AU - Chen, Yuwei

AU - Liu, Wang

AU - Shen, Jun

AU - Zhang, Guochun

AU - Tu, Heng

PY - 2021/12/15

Y1 - 2021/12/15

N2 - A new flux, Li2B4O7 − MoO3, has been successfully used to grow La2CaB10O19 (LCB) single crystals by the top seeded solution growth (TSSG) method. The suitable region for LCB crystal growth was investigated by growth experiments, and measurements of volatility and viscosity, which confirmed that the appropriate molar ratios of LCB: Li2B4O7: MoO3 are 1: 2.3: (1–1.5). The characterizations, including X-ray rocking curve, transmission spectra, optical weak absorption, and laser-induced damage threshold, have been performed on the as-grown crystal, which indicated that the LCB crystal grown from new LCB − Li2B4O7 − MoO3 system exhibits high optical quality.

AB - A new flux, Li2B4O7 − MoO3, has been successfully used to grow La2CaB10O19 (LCB) single crystals by the top seeded solution growth (TSSG) method. The suitable region for LCB crystal growth was investigated by growth experiments, and measurements of volatility and viscosity, which confirmed that the appropriate molar ratios of LCB: Li2B4O7: MoO3 are 1: 2.3: (1–1.5). The characterizations, including X-ray rocking curve, transmission spectra, optical weak absorption, and laser-induced damage threshold, have been performed on the as-grown crystal, which indicated that the LCB crystal grown from new LCB − Li2B4O7 − MoO3 system exhibits high optical quality.

KW - A1. Characterization

KW - A2. Top seeded solution growth

KW - B1. Lanthanum calcium borates

KW - B2. Nonlinear optical materials

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U2 - 10.1016/j.jcrysgro.2021.126383

DO - 10.1016/j.jcrysgro.2021.126383

M3 - Article

AN - SCOPUS:85117614437

SN - 0022-0248

VL - 576

JO - Journal of Crystal Growth

JF - Journal of Crystal Growth

M1 - 126383

ER -

Growth and characterizations of La2CaB10O19 crystal from the new Li2B4O7−MoO3 flux system with lower volatility and viscosity

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Growth and characterizations of La₂CaB₁₀O₁₉ crystal from the new Li₂B₄O₇−MoO₃ flux system with lower volatility and viscosity