AIBN-Promoted Synthesis of Bibenzo[ b][1,4]thiazines by the Condensation of 2,2′-Dithiodianiline with Methyl Aryl Ketones

Xianqiang Huang, Nianxin Rong, Pengfei Li*, Guodong Shen, Qiang Li, Nana Xin, Chuansheng Cui, Jichui Cui, Bingchuan Yang, Dacheng Li, Changqiu Zhao, Jianmin Dou, Bo Wang

*此作品的通讯作者

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摘要

A series of bibenzo[b][1,4]thiazines with various functional groups has been synthesized by a free-radical condensation reaction. Bibenzo[b][1,4]thiazines were obtained in moderate to good yield (up to 85%) through a one-step reaction of readily available 2,2′-dithiodianiline and methyl aryl ketones with AIBN as radical initiator in HOAc. Bibenzo[b][1,4]thiazines exhibit diversiform solid-state packing.

源语言英语
页(从-至)3332-3336
页数5
期刊Organic Letters
20
11
DOI
出版状态已出版 - 1 6月 2018

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Huang, X., Rong, N., Li, P., Shen, G., Li, Q., Xin, N., Cui, C., Cui, J., Yang, B., Li, D., Zhao, C., Dou, J., & Wang, B. (2018). AIBN-Promoted Synthesis of Bibenzo[ b][1,4]thiazines by the Condensation of 2,2′-Dithiodianiline with Methyl Aryl Ketones. Organic Letters, 20(11), 3332-3336. https://doi.org/10.1021/acs.orglett.8b01238