6′-Methyl-1′,2′,3′,4′-tetra-hydro-spiro- cyclo-hexane-2′-quinazolin-4′-one

Zhang Ling; Daxin Shi; Fan Yanqiu; Xia Wei; Jiarong Li

doi:10.1107/S1600536809014111

6′-Methyl-1′,2′,3′,4′-tetra-hydro-spiro- cyclo-hexane-2′-quinazolin-4′-one

Zhang Ling, Daxin Shi, Fan Yanqiu, Xia Wei, Jiarong Li^*

^*此作品的通讯作者

化学与化工学院

Beijing Institute of Technology

科研成果: 期刊稿件 › 文章 › 同行评审

1 引用（Scopus）

摘要

The title compound, C14H18N2O, was synthesized by the reaction of cyclo-hexa-none and 2-amino-5-methyl-benzonitrile. In the mol-ecule, the cyclo-hexane ring displays a chair conformation, whereas the 1,3-diaza-cyclo-hexane moiety of the bicyclic system has a sofa conformation with the spiro C atom displaced by 0.603 (2) Å from the rest of the atoms of the 1,3-diaza-cyclo-hexane ring [planar within 0.052 (2) Å]. Mol-ecules are linked into centrosymmetric dimers via N - H⋯O hydrogen bonds.

源语言	英语
页（从-至）	o1097
期刊	Acta Crystallographica Section E: Structure Reports Online
卷	65
期	5
DOI	https://doi.org/10.1107/S1600536809014111
出版状态	已出版 - 2009

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Ling, Z., Shi, D., Yanqiu, F., Wei, X., & Li, J. (2009). 6′-Methyl-1′,2′,3′,4′-tetra-hydro-spiro- cyclo-hexane-2′-quinazolin-4′-one. Acta Crystallographica Section E: Structure Reports Online, 65(5), o1097. https://doi.org/10.1107/S1600536809014111

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title = "6′-Methyl-1′,2′,3′,4′-tetra-hydro-spiro- cyclo-hexane-2′-quinazolin-4′-one",

abstract = "The title compound, C14H18N2O, was synthesized by the reaction of cyclo-hexa-none and 2-amino-5-methyl-benzonitrile. In the mol-ecule, the cyclo-hexane ring displays a chair conformation, whereas the 1,3-diaza-cyclo-hexane moiety of the bicyclic system has a sofa conformation with the spiro C atom displaced by 0.603 (2) {\AA} from the rest of the atoms of the 1,3-diaza-cyclo-hexane ring [planar within 0.052 (2) {\AA}]. Mol-ecules are linked into centrosymmetric dimers via N - H⋯O hydrogen bonds.",

author = "Zhang Ling and Daxin Shi and Fan Yanqiu and Xia Wei and Jiarong Li",

year = "2009",

doi = "10.1107/S1600536809014111",

language = "English",

volume = "65",

pages = "o1097",

journal = "Acta Crystallographica Section E: Structure Reports Online",

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T1 - 6′-Methyl-1′,2′,3′,4′-tetra-hydro-spiro- cyclo-hexane-2′-quinazolin-4′-one

AU - Ling, Zhang

AU - Shi, Daxin

AU - Yanqiu, Fan

AU - Wei, Xia

AU - Li, Jiarong

PY - 2009

Y1 - 2009

N2 - The title compound, C14H18N2O, was synthesized by the reaction of cyclo-hexa-none and 2-amino-5-methyl-benzonitrile. In the mol-ecule, the cyclo-hexane ring displays a chair conformation, whereas the 1,3-diaza-cyclo-hexane moiety of the bicyclic system has a sofa conformation with the spiro C atom displaced by 0.603 (2) Å from the rest of the atoms of the 1,3-diaza-cyclo-hexane ring [planar within 0.052 (2) Å]. Mol-ecules are linked into centrosymmetric dimers via N - H⋯O hydrogen bonds.

AB - The title compound, C14H18N2O, was synthesized by the reaction of cyclo-hexa-none and 2-amino-5-methyl-benzonitrile. In the mol-ecule, the cyclo-hexane ring displays a chair conformation, whereas the 1,3-diaza-cyclo-hexane moiety of the bicyclic system has a sofa conformation with the spiro C atom displaced by 0.603 (2) Å from the rest of the atoms of the 1,3-diaza-cyclo-hexane ring [planar within 0.052 (2) Å]. Mol-ecules are linked into centrosymmetric dimers via N - H⋯O hydrogen bonds.

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U2 - 10.1107/S1600536809014111

DO - 10.1107/S1600536809014111

M3 - Article

AN - SCOPUS:66749162689

SN - 1600-5368

VL - 65

SP - o1097

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 5

ER -

6′-Methyl-1′,2′,3′,4′-tetra-hydro-spiro- cyclo-hexane-2′-quinazolin-4′-one

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