4,5,6-Tri-O-acetyl-2,3-di-S-ethyl-2,3-dithio-d-allose diethyl dithio-acetal

Xiao Dong Xi; Da Xin Shi; Hui Li; Yun Zheng Li; Qin Pei Wu

doi:10.1107/S1600536809015694

4,5,6-Tri-O-acetyl-2,3-di-S-ethyl-2,3-dithio-d-allose diethyl dithio-acetal

Xiao Dong Xi, Da Xin Shi, Hui Li, Yun Zheng Li, Qin Pei Wu^*

^*此作品的通讯作者

化学与化工学院

Beijing Institute of Technology

科研成果: 期刊稿件 › 文章 › 同行评审

2 引用（Scopus）

摘要

The title compound, C₂₀H₃₆O₆S₄, was obtained by ethanethiol-ysis of 3,5,6-tri-O-acetyl-1,2-O-isopropyl-idene - d-gluco-furan - ose. One of the ethyl groups is disordered over two sites with refined occupancies of 0.869 (6) and 0.131 (6). Compared with the precursor, the absolute configuration of the stereocenters at positions C-3 and C-2 are inverted and maintained, respectively.

源语言	英语
页（从-至）	o1227
期刊	Acta Crystallographica Section E: Structure Reports Online
卷	65
期	6
DOI	https://doi.org/10.1107/S1600536809015694
出版状态	已出版 - 2009

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10.1107/S1600536809015694

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Xi, X. D., Shi, D. X., Li, H., Li, Y. Z., & Wu, Q. P. (2009). 4,5,6-Tri-O-acetyl-2,3-di-S-ethyl-2,3-dithio-d-allose diethyl dithio-acetal. Acta Crystallographica Section E: Structure Reports Online, 65(6), o1227. https://doi.org/10.1107/S1600536809015694

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title = "4,5,6-Tri-O-acetyl-2,3-di-S-ethyl-2,3-dithio-d-allose diethyl dithio-acetal",

abstract = "The title compound, C20H36O6S4, was obtained by ethanethiol-ysis of 3,5,6-tri-O-acetyl-1,2-O-isopropyl-idene - d-gluco-furan - ose. One of the ethyl groups is disordered over two sites with refined occupancies of 0.869 (6) and 0.131 (6). Compared with the precursor, the absolute configuration of the stereocenters at positions C-3 and C-2 are inverted and maintained, respectively.",

author = "Xi, {Xiao Dong} and Shi, {Da Xin} and Hui Li and Li, {Yun Zheng} and Wu, {Qin Pei}",

year = "2009",

doi = "10.1107/S1600536809015694",

language = "English",

volume = "65",

pages = "o1227",

journal = "Acta Crystallographica Section E: Structure Reports Online",

issn = "1600-5368",

publisher = "International Union of Crystallography",

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TY - JOUR

T1 - 4,5,6-Tri-O-acetyl-2,3-di-S-ethyl-2,3-dithio-d-allose diethyl dithio-acetal

AU - Xi, Xiao Dong

AU - Shi, Da Xin

AU - Li, Hui

AU - Li, Yun Zheng

AU - Wu, Qin Pei

PY - 2009

Y1 - 2009

N2 - The title compound, C20H36O6S4, was obtained by ethanethiol-ysis of 3,5,6-tri-O-acetyl-1,2-O-isopropyl-idene - d-gluco-furan - ose. One of the ethyl groups is disordered over two sites with refined occupancies of 0.869 (6) and 0.131 (6). Compared with the precursor, the absolute configuration of the stereocenters at positions C-3 and C-2 are inverted and maintained, respectively.

AB - The title compound, C20H36O6S4, was obtained by ethanethiol-ysis of 3,5,6-tri-O-acetyl-1,2-O-isopropyl-idene - d-gluco-furan - ose. One of the ethyl groups is disordered over two sites with refined occupancies of 0.869 (6) and 0.131 (6). Compared with the precursor, the absolute configuration of the stereocenters at positions C-3 and C-2 are inverted and maintained, respectively.

UR - http://www.scopus.com/inward/record.url?scp=67649878580&partnerID=8YFLogxK

U2 - 10.1107/S1600536809015694

DO - 10.1107/S1600536809015694

M3 - Article

AN - SCOPUS:67649878580

SN - 1600-5368

VL - 65

SP - o1227

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 6

ER -

4,5,6-Tri-O-acetyl-2,3-di-S-ethyl-2,3-dithio-d-allose diethyl dithio-acetal

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