TY - JOUR
T1 - The synthesis of SbSI rodlike crystals with studded pyramids
AU - Yang, Qing
AU - Tang, Kaibin
AU - Wang, Chunrui
AU - Hai, Bin
AU - Shen, Guozhen
AU - An, Changhua
AU - Zhang, Chunjuan
AU - Qian, Yitai
PY - 2001/12
Y1 - 2001/12
N2 - The SbSI rodlike crystals with studded pyramids were synthesized from the reaction among antimony trichloride, thiourea, and excessive sodium iodide under moderate hydrothermal conditions at 200°C. The final products were characterized by XRD, SEM, XPS, and elemental analysis. The SEM images showed the SbSI rodlike crystals are inserted some octahedrons on the surfaces of the rods. Typically, the structure is 3-4mm in length, 8-10μm in diameter for a singular crystal. The size of the pyramids on the surface is about 10μm in height and the length of hemline is 6-12μm.
AB - The SbSI rodlike crystals with studded pyramids were synthesized from the reaction among antimony trichloride, thiourea, and excessive sodium iodide under moderate hydrothermal conditions at 200°C. The final products were characterized by XRD, SEM, XPS, and elemental analysis. The SEM images showed the SbSI rodlike crystals are inserted some octahedrons on the surfaces of the rods. Typically, the structure is 3-4mm in length, 8-10μm in diameter for a singular crystal. The size of the pyramids on the surface is about 10μm in height and the length of hemline is 6-12μm.
KW - A1. x-ray diffraction
KW - A2. hydrothermal crystal growth
KW - B1. inorganic compounds
UR - http://www.scopus.com/inward/record.url?scp=0035546556&partnerID=8YFLogxK
U2 - 10.1016/S0022-0248(01)01643-8
DO - 10.1016/S0022-0248(01)01643-8
M3 - Article
AN - SCOPUS:0035546556
SN - 0022-0248
VL - 233
SP - 774
EP - 778
JO - Journal of Crystal Growth
JF - Journal of Crystal Growth
IS - 4
ER -