The synthesis of SbSI rodlike crystals with studded pyramids

Qing Yang; Kaibin Tang; Chunrui Wang; Bin Hai; Guozhen Shen; Changhua An; Chunjuan Zhang; Yitai Qian

doi:10.1016/S0022-0248(01)01643-8

The synthesis of SbSI rodlike crystals with studded pyramids

Qing Yang, Kaibin Tang, Chunrui Wang, Bin Hai, Guozhen Shen, Changhua An, Chunjuan Zhang, Yitai Qian

University of Science and Technology of China

Research output: Contribution to journal › Article › peer-review

15 Citations (Scopus)

Abstract

The SbSI rodlike crystals with studded pyramids were synthesized from the reaction among antimony trichloride, thiourea, and excessive sodium iodide under moderate hydrothermal conditions at 200°C. The final products were characterized by XRD, SEM, XPS, and elemental analysis. The SEM images showed the SbSI rodlike crystals are inserted some octahedrons on the surfaces of the rods. Typically, the structure is 3-4mm in length, 8-10μm in diameter for a singular crystal. The size of the pyramids on the surface is about 10μm in height and the length of hemline is 6-12μm.

Original language	English
Pages (from-to)	774-778
Number of pages	5
Journal	Journal of Crystal Growth
Volume	233
Issue number	4
DOIs	https://doi.org/10.1016/S0022-0248(01)01643-8
Publication status	Published - Dec 2001
Externally published	Yes

Keywords

A1. x-ray diffraction
A2. hydrothermal crystal growth
B1. inorganic compounds

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10.1016/S0022-0248(01)01643-8

Cite this

Yang, Q., Tang, K., Wang, C., Hai, B., Shen, G., An, C., Zhang, C., & Qian, Y. (2001). The synthesis of SbSI rodlike crystals with studded pyramids. Journal of Crystal Growth, 233(4), 774-778. https://doi.org/10.1016/S0022-0248(01)01643-8

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abstract = "The SbSI rodlike crystals with studded pyramids were synthesized from the reaction among antimony trichloride, thiourea, and excessive sodium iodide under moderate hydrothermal conditions at 200°C. The final products were characterized by XRD, SEM, XPS, and elemental analysis. The SEM images showed the SbSI rodlike crystals are inserted some octahedrons on the surfaces of the rods. Typically, the structure is 3-4mm in length, 8-10μm in diameter for a singular crystal. The size of the pyramids on the surface is about 10μm in height and the length of hemline is 6-12μm.",

keywords = "A1. x-ray diffraction, A2. hydrothermal crystal growth, B1. inorganic compounds",

author = "Qing Yang and Kaibin Tang and Chunrui Wang and Bin Hai and Guozhen Shen and Changhua An and Chunjuan Zhang and Yitai Qian",

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doi = "10.1016/S0022-0248(01)01643-8",

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T1 - The synthesis of SbSI rodlike crystals with studded pyramids

AU - Yang, Qing

AU - Tang, Kaibin

AU - Wang, Chunrui

AU - Hai, Bin

AU - Shen, Guozhen

AU - An, Changhua

AU - Zhang, Chunjuan

AU - Qian, Yitai

PY - 2001/12

Y1 - 2001/12

N2 - The SbSI rodlike crystals with studded pyramids were synthesized from the reaction among antimony trichloride, thiourea, and excessive sodium iodide under moderate hydrothermal conditions at 200°C. The final products were characterized by XRD, SEM, XPS, and elemental analysis. The SEM images showed the SbSI rodlike crystals are inserted some octahedrons on the surfaces of the rods. Typically, the structure is 3-4mm in length, 8-10μm in diameter for a singular crystal. The size of the pyramids on the surface is about 10μm in height and the length of hemline is 6-12μm.

AB - The SbSI rodlike crystals with studded pyramids were synthesized from the reaction among antimony trichloride, thiourea, and excessive sodium iodide under moderate hydrothermal conditions at 200°C. The final products were characterized by XRD, SEM, XPS, and elemental analysis. The SEM images showed the SbSI rodlike crystals are inserted some octahedrons on the surfaces of the rods. Typically, the structure is 3-4mm in length, 8-10μm in diameter for a singular crystal. The size of the pyramids on the surface is about 10μm in height and the length of hemline is 6-12μm.

KW - A1. x-ray diffraction

KW - A2. hydrothermal crystal growth

KW - B1. inorganic compounds

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The synthesis of SbSI rodlike crystals with studded pyramids

Abstract

Keywords

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