TY - JOUR
T1 - The synthesis and characterization of nanocrystalline Cu- and Ag-based multinary sulfide semiconductors
AU - An, Changhua
AU - Tang, Kaibin
AU - Shen, Guozhen
AU - Wang, Chunrui
AU - Huang, Liying
AU - Qian, Yitai
PY - 2003/4/30
Y1 - 2003/4/30
N2 - The novel polygonal flake like Ag8SnS6 crystal, Cu2FeSnS4 flaky, and well-dispersed Cu2CoSnS4 nanoparticles were successfully prepared via a convenient hydrothermal reaction route at relatively low temperature, which was avoiding the use of high temperature treatments or toxic organic solvents. The products were characterized by means of X-ray powder diffraction (XRD), transmission electronic microscopy (TEM), X-ray photoelectronic spectra (XPS) and inductively coupled plasma-atomic emission spectroscopy (ICP-AES). It was found that the reaction temperature played a key role for the formation of the target products.
AB - The novel polygonal flake like Ag8SnS6 crystal, Cu2FeSnS4 flaky, and well-dispersed Cu2CoSnS4 nanoparticles were successfully prepared via a convenient hydrothermal reaction route at relatively low temperature, which was avoiding the use of high temperature treatments or toxic organic solvents. The products were characterized by means of X-ray powder diffraction (XRD), transmission electronic microscopy (TEM), X-ray photoelectronic spectra (XPS) and inductively coupled plasma-atomic emission spectroscopy (ICP-AES). It was found that the reaction temperature played a key role for the formation of the target products.
KW - A. Chalcogenides
KW - A. Nanostructure
KW - B. Chemical synthesis
KW - C. X-ray diffraction
UR - http://www.scopus.com/inward/record.url?scp=0038558418&partnerID=8YFLogxK
U2 - 10.1016/S0025-5408(03)00046-1
DO - 10.1016/S0025-5408(03)00046-1
M3 - Article
AN - SCOPUS:0038558418
SN - 0025-5408
VL - 38
SP - 823
EP - 830
JO - Materials Research Bulletin
JF - Materials Research Bulletin
IS - 5
ER -