Synthesis technique of 2-methyl-6-nitroaniline

Lei Qi; Si Ping Pang; Cheng Hui Sun

Synthesis technique of 2-methyl-6-nitroaniline

Lei Qi, Si Ping Pang^*, Cheng Hui Sun

^*Corresponding author for this work

School of Material Science and Engineering

Beijing Institute of Technology

Research output: Contribution to journal › Article › peer-review

6 Citations (Scopus)

Abstract

The synthesis technique of 2-methyl-6-nitroaniline was studied. In previous method, acetylation and nitration of 2-methyla-niline were completed in one pot, but the nitration reaction temperature was difficult to be controlled. To improve the method, the acetylation and nitration were detached into two parts. The structure of the product, its by-product and its intermediate were characterized by IR,NMR and MS. The results show that the temperature of nitration process can be controlled easily, and the yield is 59.4% and the purity is up to 99.68%.

Original language	English
Pages (from-to)	4-6+10
Journal	Hanneng Cailiao/Chinese Journal of Energetic Materials
Volume	17
Issue number	1
Publication status	Published - Feb 2009

Keywords

2-methyl-4-nitroaniline
Organic chemistry
Synthesis

Cite this

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title = "Synthesis technique of 2-methyl-6-nitroaniline",

abstract = "The synthesis technique of 2-methyl-6-nitroaniline was studied. In previous method, acetylation and nitration of 2-methyla-niline were completed in one pot, but the nitration reaction temperature was difficult to be controlled. To improve the method, the acetylation and nitration were detached into two parts. The structure of the product, its by-product and its intermediate were characterized by IR,NMR and MS. The results show that the temperature of nitration process can be controlled easily, and the yield is 59.4% and the purity is up to 99.68%.",

keywords = "2-methyl-4-nitroaniline, Organic chemistry, Synthesis",

author = "Lei Qi and Pang, {Si Ping} and Sun, {Cheng Hui}",

year = "2009",

month = feb,

language = "English",

volume = "17",

pages = "4--6+10",

journal = "Hanneng Cailiao/Chinese Journal of Energetic Materials",

issn = "1006-9941",

publisher = "Institute of Chemical Materials, China Academy of Engineering Physics",

number = "1",

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TY - JOUR

T1 - Synthesis technique of 2-methyl-6-nitroaniline

AU - Qi, Lei

AU - Pang, Si Ping

AU - Sun, Cheng Hui

PY - 2009/2

Y1 - 2009/2

N2 - The synthesis technique of 2-methyl-6-nitroaniline was studied. In previous method, acetylation and nitration of 2-methyla-niline were completed in one pot, but the nitration reaction temperature was difficult to be controlled. To improve the method, the acetylation and nitration were detached into two parts. The structure of the product, its by-product and its intermediate were characterized by IR,NMR and MS. The results show that the temperature of nitration process can be controlled easily, and the yield is 59.4% and the purity is up to 99.68%.

AB - The synthesis technique of 2-methyl-6-nitroaniline was studied. In previous method, acetylation and nitration of 2-methyla-niline were completed in one pot, but the nitration reaction temperature was difficult to be controlled. To improve the method, the acetylation and nitration were detached into two parts. The structure of the product, its by-product and its intermediate were characterized by IR,NMR and MS. The results show that the temperature of nitration process can be controlled easily, and the yield is 59.4% and the purity is up to 99.68%.

KW - 2-methyl-4-nitroaniline

KW - Organic chemistry

KW - Synthesis

UR - http://www.scopus.com/inward/record.url?scp=62749090136&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:62749090136

SN - 1006-9941

VL - 17

SP - 4-6+10

JO - Hanneng Cailiao/Chinese Journal of Energetic Materials

JF - Hanneng Cailiao/Chinese Journal of Energetic Materials

IS - 1

ER -

Synthesis technique of 2-methyl-6-nitroaniline

Abstract

Keywords

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