Synthesis and characterization of phenyl(1,3,6,8-tetraazatricyclo[4.3.1. 13,8]undecan-4-YL)-methanone and its derivatives

Cong Liu; Rongji Dai; Guowei Yao; Yulin Deng

doi:10.3987/COM-13-12897

Synthesis and characterization of phenyl(1,3,6,8-tetraazatricyclo[4.3.1. 1^3,8]undecan-4-YL)-methanone and its derivatives

Cong Liu, Rongji Dai^*, Guowei Yao, Yulin Deng

^*Corresponding author for this work

Beijing Institute of Technology

Research output: Contribution to journal › Article › peer-review

Abstract

A quick and highly efficient method for the synthesis of phenyl(1,3,6,8-tetraazatricyclo[4.3.1.1^3,8]undecan-4-yl)methanone and its derivatives from hexamine and 2-bromo-1-arylethanones has been established via a Stevens rearrangement. Structures of the products were characterized by NMR and X-ray crystallography.

Original language	English
Pages (from-to)	627-630
Number of pages	4
Journal	Heterocycles
Volume	89
Issue number	3
DOIs	https://doi.org/10.3987/COM-13-12897
Publication status	Published - 2014

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Liu, C., Dai, R., Yao, G., & Deng, Y. (2014). Synthesis and characterization of phenyl(1,3,6,8-tetraazatricyclo[4.3.1. 1^3,8]undecan-4-YL)-methanone and its derivatives. Heterocycles, 89(3), 627-630. https://doi.org/10.3987/COM-13-12897

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AU - Yao, Guowei

AU - Deng, Yulin

PY - 2014

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AB - A quick and highly efficient method for the synthesis of phenyl(1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecan-4-yl)methanone and its derivatives from hexamine and 2-bromo-1-arylethanones has been established via a Stevens rearrangement. Structures of the products were characterized by NMR and X-ray crystallography.

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Synthesis and characterization of phenyl(1,3,6,8-tetraazatricyclo[4.3.1. 1^3,8]undecan-4-YL)-methanone and its derivatives

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