Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries

Ming Yue Zhou; Xiao Qing Ding; Li Peng Hou; Jin Xie; Bo Quan Li; Jia Qi Huang; Xue Qiang Zhang; Qiang Zhang

doi:10.1016/j.xpro.2022.101867

Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries

Ming Yue Zhou, Xiao Qing Ding, Li Peng Hou, Jin Xie, Bo Quan Li, Jia Qi Huang, Xue Qiang Zhang^*, Qiang Zhang^*

^*Corresponding author for this work

Advanced Research Institute of Multidisciplinary Science

Research output: Contribution to journal › Article › peer-review

2 Citations (Scopus)

Abstract

In this protocol, we describe the quantification of electrolytes using nuclear magnetic resonance. We detail the steps involved for battery cycling, sample preparation, instrument operation, and data analysis. The protocol can be used to quantify electrolyte decomposition reactions and the apparent electron transfer numbers of different electrolyte components. The protocol is optimized for lithium-based anode-free batteries but can also be applied to other rechargeable batteries. For complete details on the use and execution of this protocol, please refer to Zhou et al. (2022).¹

Original language	English
Article number	101867
Journal	STAR Protocols
Volume	3
Issue number	4
DOIs	https://doi.org/10.1016/j.xpro.2022.101867
Publication status	Published - 16 Dec 2022

Keywords

Chemistry
Energy
Material sciences
NMR

Access to Document

10.1016/j.xpro.2022.101867

Cite this

@article{d50a350510c6443cbdd18d54405f11d2,

title = "Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries",

abstract = "In this protocol, we describe the quantification of electrolytes using nuclear magnetic resonance. We detail the steps involved for battery cycling, sample preparation, instrument operation, and data analysis. The protocol can be used to quantify electrolyte decomposition reactions and the apparent electron transfer numbers of different electrolyte components. The protocol is optimized for lithium-based anode-free batteries but can also be applied to other rechargeable batteries. For complete details on the use and execution of this protocol, please refer to Zhou et al. (2022).1",

keywords = "Chemistry, Energy, Material sciences, NMR",

author = "Zhou, {Ming Yue} and Ding, {Xiao Qing} and Hou, {Li Peng} and Jin Xie and Li, {Bo Quan} and Huang, {Jia Qi} and Zhang, {Xue Qiang} and Qiang Zhang",

note = "Publisher Copyright: {\textcopyright} 2022 The Author(s)",

year = "2022",

month = dec,

day = "16",

doi = "10.1016/j.xpro.2022.101867",

language = "English",

volume = "3",

journal = "STAR Protocols",

issn = "2666-1667",

publisher = "Cell Press",

number = "4",

}

TY - JOUR

T1 - Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries

AU - Zhou, Ming Yue

AU - Ding, Xiao Qing

AU - Hou, Li Peng

AU - Xie, Jin

AU - Li, Bo Quan

AU - Huang, Jia Qi

AU - Zhang, Xue Qiang

AU - Zhang, Qiang

PY - 2022/12/16

Y1 - 2022/12/16

N2 - In this protocol, we describe the quantification of electrolytes using nuclear magnetic resonance. We detail the steps involved for battery cycling, sample preparation, instrument operation, and data analysis. The protocol can be used to quantify electrolyte decomposition reactions and the apparent electron transfer numbers of different electrolyte components. The protocol is optimized for lithium-based anode-free batteries but can also be applied to other rechargeable batteries. For complete details on the use and execution of this protocol, please refer to Zhou et al. (2022).1

AB - In this protocol, we describe the quantification of electrolytes using nuclear magnetic resonance. We detail the steps involved for battery cycling, sample preparation, instrument operation, and data analysis. The protocol can be used to quantify electrolyte decomposition reactions and the apparent electron transfer numbers of different electrolyte components. The protocol is optimized for lithium-based anode-free batteries but can also be applied to other rechargeable batteries. For complete details on the use and execution of this protocol, please refer to Zhou et al. (2022).1

KW - Chemistry

KW - Energy

KW - Material sciences

KW - NMR

UR - http://www.scopus.com/inward/record.url?scp=85142184800&partnerID=8YFLogxK

U2 - 10.1016/j.xpro.2022.101867

DO - 10.1016/j.xpro.2022.101867

M3 - Article

C2 - 36595950

AN - SCOPUS:85142184800

SN - 2666-1667

VL - 3

JO - STAR Protocols

JF - STAR Protocols

IS - 4

M1 - 101867

ER -

Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this