Probing hydrogen effect on nanomechanical properties of X65 pipeline steel using in-situ electrochemical nanoindentation

Dong Wang, Anette Brocks Hagen, Di Wan, Xu Lu*, Roy Johnsen

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

19 Citations (Scopus)

Abstract

The hydrogen effect on a X65 carbon steel was investigated using in-situ electrochemical nanoindentation approach. The alterations in elastic behavior, pop-in load, and hardness under hydrogen-free and hydrogen-charged conditions in both ferrite and bainite were compared and discussed. The results demonstrated a non-affected elastic behavior by hydrogen in both microconstituents. The homogeneous and heterogeneous dislocation nucleation are proposed as the dominant mechanisms for pop-in behavior in ferrite and bainite, respectively. In addition, the reduction of pop-in load by hydrogen in both microconstituents indicates a hydrogen-enhanced dislocation nucleation in both homogenous and heterogeneous manners. Moreover, a hydrogen-induced hardness increment was detected in both microconstituents, which is related to the hydrogen-enhanced lattice friction on dislocations. Also, the more prominent hardness increment in bainite was caused by its significantly more trapping sites.

Original languageEnglish
Article number141819
JournalMaterials Science and Engineering: A
Volume824
DOIs
Publication statusPublished - 8 Sept 2021
Externally publishedYes

Keywords

  • Carbon steel
  • Dislocation
  • Hydrogen embrittlement
  • In-situ test
  • Nanoindentation

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