Preparation of β-TCP/HAP biphasic porous bioceramic

Chao Bang Guo; Hai Bo Jin; Guang Long Li; Yun Yang; Ming Kui Du; Ke Ya Mao

Preparation of β-TCP/HAP biphasic porous bioceramic

Chao Bang Guo, Hai Bo Jin^*, Guang Long Li, Yun Yang, Ming Kui Du, Ke Ya Mao

^*Corresponding author for this work

School of Material Science and Engineering

Research output: Contribution to journal › Article › peer-review

Abstract

β-TCP/HAP biphasic bioceramic with good bioactivity and natural porous bone structure was fabricated by heating calcined bovine cancellouse bone with different quantities of NH₄H₂PO₄ and sintered temperature. The crystalline phases and microstructure of specimens were determined by the XRD scanning electron microscope (SEM). The results revealed that the obtained β-TCP/HAP biphasic porous bioceramic with dimensions of 200~800μm macropores and 1~5μm micropores exhibited good biological activity and biodegradability. With NH₄H₂PO₄ increasing in the calcined bovine bone, HAP would gradually convert into different crystalline phase compositions of TCP/HAP, TCP/HAP/Ca₂P₂O₇ at high temperature. Similarly, raising the heating temperature, TCP would also gradually convert into Ca₂P₂O₇. These results suggest that use different quantities of NH₄H₂PO₄ as addition could improve the repeatability, precision and creditability of the study.

Original language	English
Pages (from-to)	263-266
Number of pages	4
Journal	Rengong Jingti Xuebao/Journal of Synthetic Crystals
Volume	38
Issue number	SUPPL. 1
Publication status	Published - Aug 2009

Keywords

Biological activity
Biphasic calcium phosphate ceramic
Low temperature calcination
Porous bioceramic

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@article{ed53f658028a443891f6608f9e27f17e,

title = "Preparation of β-TCP/HAP biphasic porous bioceramic",

abstract = "β-TCP/HAP biphasic bioceramic with good bioactivity and natural porous bone structure was fabricated by heating calcined bovine cancellouse bone with different quantities of NH4H2PO4 and sintered temperature. The crystalline phases and microstructure of specimens were determined by the XRD scanning electron microscope (SEM). The results revealed that the obtained β-TCP/HAP biphasic porous bioceramic with dimensions of 200~800μm macropores and 1~5μm micropores exhibited good biological activity and biodegradability. With NH4H2PO4 increasing in the calcined bovine bone, HAP would gradually convert into different crystalline phase compositions of TCP/HAP, TCP/HAP/Ca2P2O7 at high temperature. Similarly, raising the heating temperature, TCP would also gradually convert into Ca2P2O7. These results suggest that use different quantities of NH4H2PO4 as addition could improve the repeatability, precision and creditability of the study.",

keywords = "Biological activity, Biphasic calcium phosphate ceramic, Low temperature calcination, Porous bioceramic",

author = "Guo, {Chao Bang} and Jin, {Hai Bo} and Li, {Guang Long} and Yun Yang and Du, {Ming Kui} and Mao, {Ke Ya}",

year = "2009",

month = aug,

language = "English",

volume = "38",

pages = "263--266",

journal = "Rengong Jingti Xuebao/Journal of Synthetic Crystals",

issn = "1000-985X",

publisher = "Chinese Ceramic Society",

number = "SUPPL. 1",

}

TY - JOUR

T1 - Preparation of β-TCP/HAP biphasic porous bioceramic

AU - Guo, Chao Bang

AU - Jin, Hai Bo

AU - Li, Guang Long

AU - Yang, Yun

AU - Du, Ming Kui

AU - Mao, Ke Ya

PY - 2009/8

Y1 - 2009/8

N2 - β-TCP/HAP biphasic bioceramic with good bioactivity and natural porous bone structure was fabricated by heating calcined bovine cancellouse bone with different quantities of NH4H2PO4 and sintered temperature. The crystalline phases and microstructure of specimens were determined by the XRD scanning electron microscope (SEM). The results revealed that the obtained β-TCP/HAP biphasic porous bioceramic with dimensions of 200~800μm macropores and 1~5μm micropores exhibited good biological activity and biodegradability. With NH4H2PO4 increasing in the calcined bovine bone, HAP would gradually convert into different crystalline phase compositions of TCP/HAP, TCP/HAP/Ca2P2O7 at high temperature. Similarly, raising the heating temperature, TCP would also gradually convert into Ca2P2O7. These results suggest that use different quantities of NH4H2PO4 as addition could improve the repeatability, precision and creditability of the study.

AB - β-TCP/HAP biphasic bioceramic with good bioactivity and natural porous bone structure was fabricated by heating calcined bovine cancellouse bone with different quantities of NH4H2PO4 and sintered temperature. The crystalline phases and microstructure of specimens were determined by the XRD scanning electron microscope (SEM). The results revealed that the obtained β-TCP/HAP biphasic porous bioceramic with dimensions of 200~800μm macropores and 1~5μm micropores exhibited good biological activity and biodegradability. With NH4H2PO4 increasing in the calcined bovine bone, HAP would gradually convert into different crystalline phase compositions of TCP/HAP, TCP/HAP/Ca2P2O7 at high temperature. Similarly, raising the heating temperature, TCP would also gradually convert into Ca2P2O7. These results suggest that use different quantities of NH4H2PO4 as addition could improve the repeatability, precision and creditability of the study.

KW - Biological activity

KW - Biphasic calcium phosphate ceramic

KW - Low temperature calcination

KW - Porous bioceramic

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M3 - Article

AN - SCOPUS:70749159138

SN - 1000-985X

VL - 38

SP - 263

EP - 266

JO - Rengong Jingti Xuebao/Journal of Synthetic Crystals

JF - Rengong Jingti Xuebao/Journal of Synthetic Crystals

IS - SUPPL. 1

ER -

Preparation of β-TCP/HAP biphasic porous bioceramic

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