Preparation and characterization of tungsten single crystals coating by chemical transport method

Yan Wei Lv, Xiao Dong Yu*, Cheng Wen Tan, Kun Song Ma, Hong Lei Ma

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

1 Citation (Scopus)

Abstract

High purity W tube is deposited on copper tube by chemical vapor deposition at atmospheric pressure. Using the high purity W tube as raw material, single-crystal W film was deposited on the single-crystal molybdenum rod by chemical transport deposition in vacuum condition. An analysis of the single-crystal characterization and crystal perfection of the W film were obtained is made by using XRD and EBSD. By using GDMS, the degree of purity of W film was determined. By conducting a test of nanoindentation and observation through SEM of the single film, relative results concerning its mechanical properties and features has been obtained. The results show that by using chemical transport deposition high, purity W single-crystal film of specific crystallographic orientation and perfect crystal can be deposited.

Original languageEnglish
Pages (from-to)258-263
Number of pages6
JournalRengong Jingti Xuebao/Journal of Synthetic Crystals
Volume39
Issue numberSUPPL.
Publication statusPublished - Jun 2010

Keywords

  • Chemical vapor deposition
  • Electron back-scatter diffraction
  • Glow discharge mass spectrometry
  • Nanoindentation
  • Tungsten single crystal coating

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