TY - JOUR
T1 - Polyol-mediated preparation of dislike (ZnSe)2·EN precursor and its conversion to ZnSe crystal with quasi-network structure
AU - Shen, Guozhen
AU - Chen, Di
AU - Tang, Kaibin
AU - Qian, Yitai
PY - 2004/5
Y1 - 2004/5
N2 - In this paper, we reported the rapid synthesis of disklike (ZnSe 2·EN precursor via a simple and convenient polyol method. Annealing the precursor in argon stream at 500 °C resulted in the formation of ZnSe crystals with unique quasi-network structure. The obtained samples were characterized by powder x-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, infrared absorbance spectra, and thermogravimetric analysis. The influence of PEG200 on the final products in the system was also discussed.
AB - In this paper, we reported the rapid synthesis of disklike (ZnSe 2·EN precursor via a simple and convenient polyol method. Annealing the precursor in argon stream at 500 °C resulted in the formation of ZnSe crystals with unique quasi-network structure. The obtained samples were characterized by powder x-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, infrared absorbance spectra, and thermogravimetric analysis. The influence of PEG200 on the final products in the system was also discussed.
UR - http://www.scopus.com/inward/record.url?scp=3142752165&partnerID=8YFLogxK
U2 - 10.1557/JMR.2004.0183
DO - 10.1557/JMR.2004.0183
M3 - Article
AN - SCOPUS:3142752165
SN - 0884-2914
VL - 19
SP - 1369
EP - 1373
JO - Journal of Materials Research
JF - Journal of Materials Research
IS - 5
ER -