Naphthalene-1,4,5,8-tetracarboxylic 1,8-anhydride

Yan Qing Xu; Da Qiang Yuan; You Fu Zhou; Ming Yan Wu; Mao Chun Hong

doi:10.1107/S1600536805009463

Naphthalene-1,4,5,8-tetracarboxylic 1,8-anhydride

Yan Qing Xu, Da Qiang Yuan, You Fu Zhou, Ming Yan Wu, Mao Chun Hong^*

^*Corresponding author for this work

CAS - Fujian Institute of Research on the Structure of Matter

Research output: Contribution to journal › Article › peer-review

4 Citations (Scopus)

Abstract

The single-crystal X-ray structure of C₁₄H₆O ₇ was analyzed. The compound was prepared by the hydrothermal reaction of SmCl₃.nH₂O and naphthalene-1,4,5,8-tetracarboxylic dianhydride in water. After heating at 433 K for 3 d and cooling to room temperature at a rate of 13 K h^-1, yellow needle-shaped crystals of the compound were obtained. In the compound, strong O-H···O hydrogen-bonding interactions between the molecules resulted in a one-dimensional chain-like supramolecular structure.

Original language	English
Pages (from-to)	o1294-o1296
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	61
Issue number	5
DOIs	https://doi.org/10.1107/S1600536805009463
Publication status	Published - May 2005
Externally published	Yes

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title = "Naphthalene-1,4,5,8-tetracarboxylic 1,8-anhydride",

abstract = "The single-crystal X-ray structure of C14H6O 7 was analyzed. The compound was prepared by the hydrothermal reaction of SmCl3.nH2O and naphthalene-1,4,5,8-tetracarboxylic dianhydride in water. After heating at 433 K for 3 d and cooling to room temperature at a rate of 13 K h-1, yellow needle-shaped crystals of the compound were obtained. In the compound, strong O-H···O hydrogen-bonding interactions between the molecules resulted in a one-dimensional chain-like supramolecular structure.",

author = "Xu, {Yan Qing} and Yuan, {Da Qiang} and Zhou, {You Fu} and Wu, {Ming Yan} and Hong, {Mao Chun}",

year = "2005",

month = may,

doi = "10.1107/S1600536805009463",

language = "English",

volume = "61",

pages = "o1294--o1296",

journal = "Acta Crystallographica Section E: Structure Reports Online",

issn = "1600-5368",

publisher = "International Union of Crystallography",

number = "5",

}

TY - JOUR

T1 - Naphthalene-1,4,5,8-tetracarboxylic 1,8-anhydride

AU - Xu, Yan Qing

AU - Yuan, Da Qiang

AU - Zhou, You Fu

AU - Wu, Ming Yan

AU - Hong, Mao Chun

PY - 2005/5

Y1 - 2005/5

N2 - The single-crystal X-ray structure of C14H6O 7 was analyzed. The compound was prepared by the hydrothermal reaction of SmCl3.nH2O and naphthalene-1,4,5,8-tetracarboxylic dianhydride in water. After heating at 433 K for 3 d and cooling to room temperature at a rate of 13 K h-1, yellow needle-shaped crystals of the compound were obtained. In the compound, strong O-H···O hydrogen-bonding interactions between the molecules resulted in a one-dimensional chain-like supramolecular structure.

AB - The single-crystal X-ray structure of C14H6O 7 was analyzed. The compound was prepared by the hydrothermal reaction of SmCl3.nH2O and naphthalene-1,4,5,8-tetracarboxylic dianhydride in water. After heating at 433 K for 3 d and cooling to room temperature at a rate of 13 K h-1, yellow needle-shaped crystals of the compound were obtained. In the compound, strong O-H···O hydrogen-bonding interactions between the molecules resulted in a one-dimensional chain-like supramolecular structure.

UR - http://www.scopus.com/inward/record.url?scp=18544375572&partnerID=8YFLogxK

U2 - 10.1107/S1600536805009463

DO - 10.1107/S1600536805009463

M3 - Article

AN - SCOPUS:18544375572

SN - 1600-5368

VL - 61

SP - o1294-o1296

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 5

ER -

Naphthalene-1,4,5,8-tetracarboxylic 1,8-anhydride

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