Cyclo-hexa-nespiro-2′-[2′,3′,6′, 7′-tetra-hydro-1′H-cyclo-penta-[d]pyrimidin]-4′(5′H)-one

Daxin Shi; Dongfeng Qian; Qi Zhang; Jiarong Li

doi:10.1107/S1600536809005388

Cyclo-hexa-nespiro-2′-[2′,3′,6′, 7′-tetra-hydro-1′H-cyclo-penta-[d]pyrimidin]-4′(5′H)-one

Daxin Shi, Dongfeng Qian, Qi Zhang, Jiarong Li^*

^*Corresponding author for this work

School of Chemistry and Chemical Engineering

Beijing Institute of Technology

Research output: Contribution to journal › Article › peer-review

1 Citation (Scopus)

Abstract

The title compound, C¹²H¹⁸N²O, was synthesized by the reaction of cyclo-hexa-none and 2-amino-cyclo-pent-1- enecarbonitrile. In the mol-ecule of the title compound, the six-carbon ring displays a chair conformation, the six-membered 1,3-diaza ring and the cyclo-pentene ring both assume envelope conformations. Supra-molecular aggregation is achieved by N - H⋯O hydrogen bonds.

Original language	English
Pages (from-to)	o615
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	65
Issue number	3
DOIs	https://doi.org/10.1107/S1600536809005388
Publication status	Published - 2009

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Shi, D., Qian, D., Zhang, Q., & Li, J. (2009). Cyclo-hexa-nespiro-2′-[2′,3′,6′, 7′-tetra-hydro-1′H-cyclo-penta-[d]pyrimidin]-4′(5′H)-one. Acta Crystallographica Section E: Structure Reports Online, 65(3), o615. https://doi.org/10.1107/S1600536809005388

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abstract = "The title compound, C12H18N2O, was synthesized by the reaction of cyclo-hexa-none and 2-amino-cyclo-pent-1- enecarbonitrile. In the mol-ecule of the title compound, the six-carbon ring displays a chair conformation, the six-membered 1,3-diaza ring and the cyclo-pentene ring both assume envelope conformations. Supra-molecular aggregation is achieved by N - H⋯O hydrogen bonds.",

author = "Daxin Shi and Dongfeng Qian and Qi Zhang and Jiarong Li",

year = "2009",

doi = "10.1107/S1600536809005388",

language = "English",

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T1 - Cyclo-hexa-nespiro-2′-[2′,3′,6′, 7′-tetra-hydro-1′H-cyclo-penta-[d]pyrimidin]-4′(5′H)-one

AU - Shi, Daxin

AU - Qian, Dongfeng

AU - Zhang, Qi

AU - Li, Jiarong

PY - 2009

Y1 - 2009

N2 - The title compound, C12H18N2O, was synthesized by the reaction of cyclo-hexa-none and 2-amino-cyclo-pent-1- enecarbonitrile. In the mol-ecule of the title compound, the six-carbon ring displays a chair conformation, the six-membered 1,3-diaza ring and the cyclo-pentene ring both assume envelope conformations. Supra-molecular aggregation is achieved by N - H⋯O hydrogen bonds.

AB - The title compound, C12H18N2O, was synthesized by the reaction of cyclo-hexa-none and 2-amino-cyclo-pent-1- enecarbonitrile. In the mol-ecule of the title compound, the six-carbon ring displays a chair conformation, the six-membered 1,3-diaza ring and the cyclo-pentene ring both assume envelope conformations. Supra-molecular aggregation is achieved by N - H⋯O hydrogen bonds.

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JF - Acta Crystallographica Section E: Structure Reports Online

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ER -

Cyclo-hexa-nespiro-2′-[2′,3′,6′, 7′-tetra-hydro-1′H-cyclo-penta-[d]pyrimidin]-4′(5′H)-one

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