A rapid route for the synthesis of submicron se and te rod-like crystals

Guozhen Shen; Di Chen; Kaibin Tang; Yitai Qian

doi:10.1016/j.materresbull.2004.07.010

A rapid route for the synthesis of submicron se and te rod-like crystals

Guozhen Shen^*, Di Chen, Kaibin Tang, Yitai Qian

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

5 Citations (Scopus)

Abstract

Submicron Se and Te rod-like crystals were successfully synthesized via a rapid polyol process by refluxing Na₂EO₃ (E=Se, Te) and (NH₃)₂S₂O₃ in ethylene glycol at 180°C for 0.5 h under vigorous stirring. The obtained samples were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM), and XPS procedures. Studies found that reaction time and temperature have great influences on the morphology of the final products.

Original language	English
Pages (from-to)	2077-2082
Number of pages	6
Journal	Materials Research Bulletin
Volume	39
Issue number	13
DOIs	https://doi.org/10.1016/j.materresbull.2004.07.010
Publication status	Published - 2 Nov 2004
Externally published	Yes

Keywords

A. Element
B. Chemical synthesis
C. X-ray diffraction
D. Microstructure

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10.1016/j.materresbull.2004.07.010

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title = "A rapid route for the synthesis of submicron se and te rod-like crystals",

abstract = "Submicron Se and Te rod-like crystals were successfully synthesized via a rapid polyol process by refluxing Na2EO3 (E=Se, Te) and (NH3)2S2O3 in ethylene glycol at 180°C for 0.5 h under vigorous stirring. The obtained samples were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM), and XPS procedures. Studies found that reaction time and temperature have great influences on the morphology of the final products.",

keywords = "A. Element, B. Chemical synthesis, C. X-ray diffraction, D. Microstructure",

author = "Guozhen Shen and Di Chen and Kaibin Tang and Yitai Qian",

year = "2004",

month = nov,

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doi = "10.1016/j.materresbull.2004.07.010",

language = "English",

volume = "39",

pages = "2077--2082",

journal = "Materials Research Bulletin",

issn = "0025-5408",

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TY - JOUR

T1 - A rapid route for the synthesis of submicron se and te rod-like crystals

AU - Shen, Guozhen

AU - Chen, Di

AU - Tang, Kaibin

AU - Qian, Yitai

PY - 2004/11/2

Y1 - 2004/11/2

N2 - Submicron Se and Te rod-like crystals were successfully synthesized via a rapid polyol process by refluxing Na2EO3 (E=Se, Te) and (NH3)2S2O3 in ethylene glycol at 180°C for 0.5 h under vigorous stirring. The obtained samples were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM), and XPS procedures. Studies found that reaction time and temperature have great influences on the morphology of the final products.

AB - Submicron Se and Te rod-like crystals were successfully synthesized via a rapid polyol process by refluxing Na2EO3 (E=Se, Te) and (NH3)2S2O3 in ethylene glycol at 180°C for 0.5 h under vigorous stirring. The obtained samples were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM), and XPS procedures. Studies found that reaction time and temperature have great influences on the morphology of the final products.

KW - A. Element

KW - B. Chemical synthesis

KW - C. X-ray diffraction

KW - D. Microstructure

UR - http://www.scopus.com/inward/record.url?scp=4644235584&partnerID=8YFLogxK

U2 - 10.1016/j.materresbull.2004.07.010

DO - 10.1016/j.materresbull.2004.07.010

M3 - Article

AN - SCOPUS:4644235584

SN - 0025-5408

VL - 39

SP - 2077

EP - 2082

JO - Materials Research Bulletin

JF - Materials Research Bulletin

IS - 13

ER -

A rapid route for the synthesis of submicron se and te rod-like crystals

Abstract

Keywords

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