The synthesis and characterization of nanocrystalline Cu- and Ag-based multinary sulfide semiconductors

Changhua An; Kaibin Tang; Guozhen Shen; Chunrui Wang; Liying Huang; Yitai Qian

doi:10.1016/S0025-5408(03)00046-1

The synthesis and characterization of nanocrystalline Cu- and Ag-based multinary sulfide semiconductors

Changhua An, Kaibin Tang^*, Guozhen Shen, Chunrui Wang, Liying Huang, Yitai Qian

^*Corresponding author for this work

University of Science and Technology of China

Research output: Contribution to journal › Article › peer-review

37 Citations (Scopus)

Abstract

The novel polygonal flake like Ag₈SnS₆ crystal, Cu₂FeSnS₄ flaky, and well-dispersed Cu₂CoSnS₄ nanoparticles were successfully prepared via a convenient hydrothermal reaction route at relatively low temperature, which was avoiding the use of high temperature treatments or toxic organic solvents. The products were characterized by means of X-ray powder diffraction (XRD), transmission electronic microscopy (TEM), X-ray photoelectronic spectra (XPS) and inductively coupled plasma-atomic emission spectroscopy (ICP-AES). It was found that the reaction temperature played a key role for the formation of the target products.

Original language	English
Pages (from-to)	823-830
Number of pages	8
Journal	Materials Research Bulletin
Volume	38
Issue number	5
DOIs	https://doi.org/10.1016/S0025-5408(03)00046-1
Publication status	Published - 30 Apr 2003
Externally published	Yes

Keywords

A. Chalcogenides
A. Nanostructure
B. Chemical synthesis
C. X-ray diffraction

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10.1016/S0025-5408(03)00046-1

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An, C., Tang, K., Shen, G., Wang, C., Huang, L., & Qian, Y. (2003). The synthesis and characterization of nanocrystalline Cu- and Ag-based multinary sulfide semiconductors. Materials Research Bulletin, 38(5), 823-830. https://doi.org/10.1016/S0025-5408(03)00046-1

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title = "The synthesis and characterization of nanocrystalline Cu- and Ag-based multinary sulfide semiconductors",

abstract = "The novel polygonal flake like Ag8SnS6 crystal, Cu2FeSnS4 flaky, and well-dispersed Cu2CoSnS4 nanoparticles were successfully prepared via a convenient hydrothermal reaction route at relatively low temperature, which was avoiding the use of high temperature treatments or toxic organic solvents. The products were characterized by means of X-ray powder diffraction (XRD), transmission electronic microscopy (TEM), X-ray photoelectronic spectra (XPS) and inductively coupled plasma-atomic emission spectroscopy (ICP-AES). It was found that the reaction temperature played a key role for the formation of the target products.",

keywords = "A. Chalcogenides, A. Nanostructure, B. Chemical synthesis, C. X-ray diffraction",

author = "Changhua An and Kaibin Tang and Guozhen Shen and Chunrui Wang and Liying Huang and Yitai Qian",

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doi = "10.1016/S0025-5408(03)00046-1",

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T1 - The synthesis and characterization of nanocrystalline Cu- and Ag-based multinary sulfide semiconductors

AU - An, Changhua

AU - Tang, Kaibin

AU - Shen, Guozhen

AU - Wang, Chunrui

AU - Huang, Liying

AU - Qian, Yitai

PY - 2003/4/30

Y1 - 2003/4/30

N2 - The novel polygonal flake like Ag8SnS6 crystal, Cu2FeSnS4 flaky, and well-dispersed Cu2CoSnS4 nanoparticles were successfully prepared via a convenient hydrothermal reaction route at relatively low temperature, which was avoiding the use of high temperature treatments or toxic organic solvents. The products were characterized by means of X-ray powder diffraction (XRD), transmission electronic microscopy (TEM), X-ray photoelectronic spectra (XPS) and inductively coupled plasma-atomic emission spectroscopy (ICP-AES). It was found that the reaction temperature played a key role for the formation of the target products.

AB - The novel polygonal flake like Ag8SnS6 crystal, Cu2FeSnS4 flaky, and well-dispersed Cu2CoSnS4 nanoparticles were successfully prepared via a convenient hydrothermal reaction route at relatively low temperature, which was avoiding the use of high temperature treatments or toxic organic solvents. The products were characterized by means of X-ray powder diffraction (XRD), transmission electronic microscopy (TEM), X-ray photoelectronic spectra (XPS) and inductively coupled plasma-atomic emission spectroscopy (ICP-AES). It was found that the reaction temperature played a key role for the formation of the target products.

KW - A. Chalcogenides

KW - A. Nanostructure

KW - B. Chemical synthesis

KW - C. X-ray diffraction

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U2 - 10.1016/S0025-5408(03)00046-1

DO - 10.1016/S0025-5408(03)00046-1

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SN - 0025-5408

VL - 38

SP - 823

EP - 830

JO - Materials Research Bulletin

JF - Materials Research Bulletin

IS - 5

ER -

The synthesis and characterization of nanocrystalline Cu- and Ag-based multinary sulfide semiconductors

Abstract

Keywords

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