Synthesis and characterization of a novel cellulose nonionic ether

Zi Qiang Shao; Kun Xu; Yong Sheng Tian; Fei Jun Wang; Ji Xun Wang

Synthesis and characterization of a novel cellulose nonionic ether

Zi Qiang Shao^*, Kun Xu, Yong Sheng Tian, Fei Jun Wang, Ji Xun Wang

^*Corresponding author for this work

School of Material Science and Engineering

Beijing Institute of Technology

Research output: Contribution to journal › Article › peer-review

1 Citation (Scopus)

Abstract

A kind of novel cellulose ether - trihydroxybutyl cellulose (THBC) was synthesized. The process includes the steam explosion treatment of cotton cellulose, alkalization, etherification and purification. Sweep electron microscope (SEM), Fourier transform infrared (FTIR) and X-ray diffraction were used to characterize the cellulose pretreated and the product. The effects of reaction conditions (temperature, time) on the molecular substitution (S_m) were discussed. To obtain a higher degree of molecular substitution, the reaction temperature is 80°C, and the reaction time is 4 h.

Original language	English
Pages (from-to)	188-191
Number of pages	4
Journal	Journal of Beijing Institute of Technology (English Edition)
Volume	14
Issue number	2
Publication status	Published - Jun 2005

Keywords

3,4-epoxy-1-bromo-2-butyl alcohol
Steam explosion
Thermoplastic
Trihydroxybutyl cellulose

Cite this

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title = "Synthesis and characterization of a novel cellulose nonionic ether",

abstract = "A kind of novel cellulose ether - trihydroxybutyl cellulose (THBC) was synthesized. The process includes the steam explosion treatment of cotton cellulose, alkalization, etherification and purification. Sweep electron microscope (SEM), Fourier transform infrared (FTIR) and X-ray diffraction were used to characterize the cellulose pretreated and the product. The effects of reaction conditions (temperature, time) on the molecular substitution (Sm) were discussed. To obtain a higher degree of molecular substitution, the reaction temperature is 80°C, and the reaction time is 4 h.",

keywords = "3,4-epoxy-1-bromo-2-butyl alcohol, Steam explosion, Thermoplastic, Trihydroxybutyl cellulose",

author = "Shao, {Zi Qiang} and Kun Xu and Tian, {Yong Sheng} and Wang, {Fei Jun} and Wang, {Ji Xun}",

year = "2005",

month = jun,

language = "English",

volume = "14",

pages = "188--191",

journal = "Journal of Beijing Institute of Technology (English Edition)",

issn = "1004-0579",

publisher = "Beijing Institute of Technology",

number = "2",

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TY - JOUR

T1 - Synthesis and characterization of a novel cellulose nonionic ether

AU - Shao, Zi Qiang

AU - Xu, Kun

AU - Tian, Yong Sheng

AU - Wang, Fei Jun

AU - Wang, Ji Xun

PY - 2005/6

Y1 - 2005/6

N2 - A kind of novel cellulose ether - trihydroxybutyl cellulose (THBC) was synthesized. The process includes the steam explosion treatment of cotton cellulose, alkalization, etherification and purification. Sweep electron microscope (SEM), Fourier transform infrared (FTIR) and X-ray diffraction were used to characterize the cellulose pretreated and the product. The effects of reaction conditions (temperature, time) on the molecular substitution (Sm) were discussed. To obtain a higher degree of molecular substitution, the reaction temperature is 80°C, and the reaction time is 4 h.

AB - A kind of novel cellulose ether - trihydroxybutyl cellulose (THBC) was synthesized. The process includes the steam explosion treatment of cotton cellulose, alkalization, etherification and purification. Sweep electron microscope (SEM), Fourier transform infrared (FTIR) and X-ray diffraction were used to characterize the cellulose pretreated and the product. The effects of reaction conditions (temperature, time) on the molecular substitution (Sm) were discussed. To obtain a higher degree of molecular substitution, the reaction temperature is 80°C, and the reaction time is 4 h.

KW - 3,4-epoxy-1-bromo-2-butyl alcohol

KW - Steam explosion

KW - Thermoplastic

KW - Trihydroxybutyl cellulose

UR - http://www.scopus.com/inward/record.url?scp=22844447058&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:22844447058

SN - 1004-0579

VL - 14

SP - 188

EP - 191

JO - Journal of Beijing Institute of Technology (English Edition)

JF - Journal of Beijing Institute of Technology (English Edition)

IS - 2

ER -

Synthesis and characterization of a novel cellulose nonionic ether

Abstract

Keywords

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