Preparation of ultra-fine La0.8Sr0.2MnO3-δ powders by low temperature combustion synthesis

Chang Jing Fu; Ke Ning Sun; Nai Qing Zhang; De Rui Zhou

Preparation of ultra-fine La_0.8Sr_0.2MnO_3-δ powders by low temperature combustion synthesis

Chang Jing Fu^*, Ke Ning Sun, Nai Qing Zhang, De Rui Zhou

^*Corresponding author for this work

Harbin Institute of Technology

Research output: Contribution to journal › Article › peer-review

3 Citations (Scopus)

Abstract

Ultra-fine La_0.8Sr_0.2MnO_3-δ (LSM) powder was prepared by low temperature combustion synthesis (LTCS), and the main procedure technical parameters, such as pH value, the amount of citrate, the concentration of the solution and the heating temperature were studied. The phase structure of the product was analyzed by X-ray diffraction, its grain size distribution and specific surface areas were measured by granularity analysis method and BET method, respectively. And the characteristics of the powder synthesized by LTCS, solid state reaction and co-precipitation were compared. Results show that LTCS method can synthesize LSM nanometer powder with particle size of 20-30 nm, which is with high purity and specific surface areas more than 11 m²/g.

Original language	English
Pages (from-to)	925-928
Number of pages	4
Journal	Gongneng Cailiao/Journal of Functional Materials
Volume	37
Issue number	6
Publication status	Published - Jun 2006
Externally published	Yes

Keywords

LaSrMnO
Low temperature combustion synthesis
Ultra-fine powder

Cite this

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title = "Preparation of ultra-fine La0.8Sr0.2MnO3-δ powders by low temperature combustion synthesis",

abstract = "Ultra-fine La0.8Sr0.2MnO3-δ (LSM) powder was prepared by low temperature combustion synthesis (LTCS), and the main procedure technical parameters, such as pH value, the amount of citrate, the concentration of the solution and the heating temperature were studied. The phase structure of the product was analyzed by X-ray diffraction, its grain size distribution and specific surface areas were measured by granularity analysis method and BET method, respectively. And the characteristics of the powder synthesized by LTCS, solid state reaction and co-precipitation were compared. Results show that LTCS method can synthesize LSM nanometer powder with particle size of 20-30 nm, which is with high purity and specific surface areas more than 11 m2/g.",

keywords = "LaSrMnO, Low temperature combustion synthesis, Ultra-fine powder",

author = "Fu, {Chang Jing} and Sun, {Ke Ning} and Zhang, {Nai Qing} and Zhou, {De Rui}",

year = "2006",

month = jun,

language = "English",

volume = "37",

pages = "925--928",

journal = "Gongneng Cailiao/Journal of Functional Materials",

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TY - JOUR

T1 - Preparation of ultra-fine La0.8Sr0.2MnO3-δ powders by low temperature combustion synthesis

AU - Fu, Chang Jing

AU - Sun, Ke Ning

AU - Zhang, Nai Qing

AU - Zhou, De Rui

PY - 2006/6

Y1 - 2006/6

N2 - Ultra-fine La0.8Sr0.2MnO3-δ (LSM) powder was prepared by low temperature combustion synthesis (LTCS), and the main procedure technical parameters, such as pH value, the amount of citrate, the concentration of the solution and the heating temperature were studied. The phase structure of the product was analyzed by X-ray diffraction, its grain size distribution and specific surface areas were measured by granularity analysis method and BET method, respectively. And the characteristics of the powder synthesized by LTCS, solid state reaction and co-precipitation were compared. Results show that LTCS method can synthesize LSM nanometer powder with particle size of 20-30 nm, which is with high purity and specific surface areas more than 11 m2/g.

AB - Ultra-fine La0.8Sr0.2MnO3-δ (LSM) powder was prepared by low temperature combustion synthesis (LTCS), and the main procedure technical parameters, such as pH value, the amount of citrate, the concentration of the solution and the heating temperature were studied. The phase structure of the product was analyzed by X-ray diffraction, its grain size distribution and specific surface areas were measured by granularity analysis method and BET method, respectively. And the characteristics of the powder synthesized by LTCS, solid state reaction and co-precipitation were compared. Results show that LTCS method can synthesize LSM nanometer powder with particle size of 20-30 nm, which is with high purity and specific surface areas more than 11 m2/g.

KW - LaSrMnO

KW - Low temperature combustion synthesis

KW - Ultra-fine powder

UR - http://www.scopus.com/inward/record.url?scp=33747425986&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:33747425986

SN - 1001-9731

VL - 37

SP - 925

EP - 928

JO - Gongneng Cailiao/Journal of Functional Materials

JF - Gongneng Cailiao/Journal of Functional Materials

IS - 6

ER -

Preparation of ultra-fine La_0.8Sr_0.2MnO_3-δ powders by low temperature combustion synthesis

Abstract

Keywords

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