Abstract
The Cu(ntp)2(H2O)4 coordination compound has been synthesized by direct method and its crystal has been cultured and characterized by X-ray single crystal structural analysis. The crystal is formulated as C16H16CuN2O16 and crystallized in monoclinic system, space group C2/c, with a=2.2665(7) nm, b=0.7068(2) nm, c=1.575 5(4) nm, β=126.42(1)°, V=2.030 8(13) nm 3, Dc=1.818 g·cm3. Based on DSC and TG-DTG analyses, the thermal decomposition mechanism of Cu(ntp) 2(H2O)4 is predicted that it loses its four coordinated water molecules followed by a large weight loss and formation of copper oxide on heating.
| Original language | English |
|---|---|
| Pages (from-to) | 995-999 |
| Number of pages | 5 |
| Journal | Chinese Journal of Inorganic Chemistry |
| Volume | 22 |
| Issue number | 6 |
| Publication status | Published - Jun 2006 |
Keywords
- Crystal structure
- Direct synthesis
- Thermal decomposition
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Guo, J. Y., Zhang, T. L., Zhang, J. G., Liu, Y. H., & Yu, K. B. (2006). Direct synthesis, crystal structures and thermal analyses of the two-dimensional Cu(ntp)2(H2O)4 crystal (ntp=2-nitroterephthalate). Chinese Journal of Inorganic Chemistry, 22(6), 995-999.