TY - JOUR
T1 - Template-assisted synthesis of Sb8O10(OH)2I2 tubular crystals under hydrothermal conditions
AU - Yang, Qing
AU - Tang, Kaibin
AU - Wang, Chunrui
AU - Li, Fuping
AU - Hai, Bin
AU - Shen, Guozhen
AU - An, Changhua
AU - Yu, Weichao
AU - Qian, Yitai
PY - 2001/11
Y1 - 2001/11
N2 - Mesoscale octaantimony decaoxide dihydroxide iodide (Sb8O10(OH)2I2) tubular crystals have been successfully synthesized for the first time through a hydrothermal route from Sb2S3, NaI and NaOH at 200°C. In the process, the Sb2S3 prismatic crystals serve as templates and play an important role in the formation of the Sb8O10(OH)2I2 tubular crystals in alkali aqueous solution. The products are characterized by X-ray powder diffraction and scanning electron microscopy. The sample has tubular prismatic structure. A typical tubule is 6-8mm in length, 30-50μm in diameter, and 5μm in thickness.
AB - Mesoscale octaantimony decaoxide dihydroxide iodide (Sb8O10(OH)2I2) tubular crystals have been successfully synthesized for the first time through a hydrothermal route from Sb2S3, NaI and NaOH at 200°C. In the process, the Sb2S3 prismatic crystals serve as templates and play an important role in the formation of the Sb8O10(OH)2I2 tubular crystals in alkali aqueous solution. The products are characterized by X-ray powder diffraction and scanning electron microscopy. The sample has tubular prismatic structure. A typical tubule is 6-8mm in length, 30-50μm in diameter, and 5μm in thickness.
KW - A1. X-ray diffraction
KW - A2. hydrothermal crystal growth
KW - B1. inorganic compounds
UR - https://www.scopus.com/pages/publications/0035501993
U2 - 10.1016/S0022-0248(01)01504-4
DO - 10.1016/S0022-0248(01)01504-4
M3 - Article
AN - SCOPUS:0035501993
SN - 0022-0248
VL - 233
SP - 287
EP - 291
JO - Journal of Crystal Growth
JF - Journal of Crystal Growth
IS - 1-2
ER -