TY - JOUR
T1 - Synthesis of new tetrazene(N-N{double bond, long}N-N)-linked bi(1,2,4-triazole)
AU - Li, Sheng Hua
AU - Pang, Si Ping
AU - Li, Xiao Tong
AU - Yu, Yong Zhong
AU - Zhao, Xin Qi
PY - 2007/10
Y1 - 2007/10
N2 - The reaction of 4-amino-1,2,4-triazole with sodium dichloroisocyanurate (SDCI) afforded new tetrazene(N-N{double bond, long}N-N)-linked bi(1,2,4-triazole) 2a in excellent yield. Increasing the molar ratio of SDCI to 4-amino-1,2,4-triazole, the chlorinated product 1,5,5′-trichloro-4,4′-azo-1,2,4-triazole (2b) was formed. These new compounds have been characterized by MS, 1H NMR, 13C NMR, and elemental analysis.
AB - The reaction of 4-amino-1,2,4-triazole with sodium dichloroisocyanurate (SDCI) afforded new tetrazene(N-N{double bond, long}N-N)-linked bi(1,2,4-triazole) 2a in excellent yield. Increasing the molar ratio of SDCI to 4-amino-1,2,4-triazole, the chlorinated product 1,5,5′-trichloro-4,4′-azo-1,2,4-triazole (2b) was formed. These new compounds have been characterized by MS, 1H NMR, 13C NMR, and elemental analysis.
KW - Synthesis
KW - Tetrazene
KW - Triazole
UR - https://www.scopus.com/pages/publications/34848827930
U2 - 10.1016/j.cclet.2007.08.018
DO - 10.1016/j.cclet.2007.08.018
M3 - Article
AN - SCOPUS:34848827930
SN - 1001-8417
VL - 18
SP - 1176
EP - 1178
JO - Chinese Chemical Letters
JF - Chinese Chemical Letters
IS - 10
ER -